trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidinamine

Base Information

Chemical Name:trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidinamine
CAS No.:950772-79-9
Molecular Formula:C₁₆H₃₂N₂O
Molecular Weight:268.443
Hs Code.:

Synonyms:trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidinamine

Suppliers and Price of trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidinamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidinamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidinamine

There total 11 articles about trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 950772-78-8
trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidone

: 950772-79-9
trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidinamine

Guidance literature:: With ammonia; hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; under 2585.81 Torr;

Reference yield:

: 3612-18-8
N-ethyl-4-piperidone

: 950772-79-9
trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidinamine

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 3 h / 0 - 30 °C

2: potassium carbonate / ethanol; water / 1 h / 80 °C

3: ammonia; hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2585.81 Torr

With ammonia; hydrogen; potassium carbonate; palladium 10% on activated carbon; In methanol; ethanol; water; acetone;

Reference yield:

: 862728-41-4
trans-1-ethyl-4-hydroxy-cyclohexanecarboxylic acid ethyl ester

: 950772-79-9
trans-1-[4-(propoxy)-1-ethylcyclohexyl]-4-piperidinamine

Guidance literature:: Multi-step reaction with 9 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 76 h / 0 - 20 °C

2: potassium carbonate / methanol / 1 h / 20 °C

3: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

4: triethylsilane; bismuth(III) bromide / acetonitrile / 0.5 h / 0 - 20 °C

5: sodium hydroxide; water / tetrahydrofuran; methanol / 50 °C

6: diphenyl phosphoryl azide; triethylamine / toluene / 0.5 h / 100 °C

7: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

8: potassium carbonate / ethanol; water / 1 h / 80 °C

9: ammonia; hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2585.81 Torr

With 1H-imidazole; hydrogenchloride; triethylsilane; sodium hydroxide; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; ammonia; water; hydrogen; bismuth(III) bromide; potassium carbonate; triethylamine; triphenylphosphine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; toluene; acetonitrile;