N-Methyl-salicyl-β-naphthylamid

Base Information

Chemical Name:N-Methyl-salicyl-β-naphthylamid
CAS No.:94905-32-5
Molecular Formula:C₁₈H₁₅NO₂
Molecular Weight:277.323
Hs Code.:

Synonyms:N-Methyl-salicyl-β-naphthylamid

Suppliers and Price of N-Methyl-salicyl-β-naphthylamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Methyl-salicyl-β-naphthylamid

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Technology Process of N-Methyl-salicyl-β-naphthylamid

There total 7 articles about N-Methyl-salicyl-β-naphthylamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: C₂₄H₁₇N₃O₇

: 94905-32-5
N-Methyl-salicyl-β-naphthylamid

Guidance literature:: With ammonium chloride; In dimethyl sulfoxide; at 50 ℃; for 3h; Electrolysis;
DOI:10.1021/acs.orglett.8b03178

Reference yield:

: 66691-27-8
2-(naphthalen-2-yloxy)-benzoic acid

: 94905-32-5
N-Methyl-salicyl-β-naphthylamid

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 3 h / 0 - 20 °C

2.1: sodium carbonate / dichloromethane; water / 2 h / 0 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

3.2: 0 - 20 °C

4.1: ammonium chloride / dimethyl sulfoxide / 3 h / 50 °C / Electrolysis

With oxalyl dichloride; sodium hydride; sodium carbonate; ammonium chloride; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; 4.1: |Smiles Aromatic Rearrangement;
DOI:10.1021/acs.orglett.8b03178

Reference yield:

: 1041593-26-3
C₁₇H₁₁NO

: 94905-32-5
N-Methyl-salicyl-β-naphthylamid

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; sodium hydroxide / ethanol / 16 h / Reflux

2.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 3 h / 0 - 20 °C

3.1: sodium carbonate / dichloromethane; water / 2 h / 0 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

4.2: 0 - 20 °C

5.1: ammonium chloride / dimethyl sulfoxide / 3 h / 50 °C / Electrolysis

With oxalyl dichloride; water; sodium hydride; sodium carbonate; ammonium chloride; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; 5.1: |Smiles Aromatic Rearrangement;
DOI:10.1021/acs.orglett.8b03178