1-(6-bromo-pyridin-3-yl)-3-(2-chloro-benzyl)-1,3-dihydro-benzoimidazol-2-ylideneamine

Base Information

Chemical Name:1-(6-bromo-pyridin-3-yl)-3-(2-chloro-benzyl)-1,3-dihydro-benzoimidazol-2-ylideneamine
CAS No.:1352874-59-9
Molecular Formula:C₁₉H₁₄BrClN₄
Molecular Weight:413.704
Hs Code.:

Synonyms:1-(6-bromo-pyridin-3-yl)-3-(2-chloro-benzyl)-1,3-dihydro-benzoimidazol-2-ylideneamine

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Chemical Property of 1-(6-bromo-pyridin-3-yl)-3-(2-chloro-benzyl)-1,3-dihydro-benzoimidazol-2-ylideneamine

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Technology Process of 1-(6-bromo-pyridin-3-yl)-3-(2-chloro-benzyl)-1,3-dihydro-benzoimidazol-2-ylideneamine

There total 5 articles about 1-(6-bromo-pyridin-3-yl)-3-(2-chloro-benzyl)-1,3-dihydro-benzoimidazol-2-ylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1352874-10-2
1-(6-chloropyridin-3-yl)-1H-benzo[d]imidazol-2-amine

: 611-17-6
1-bromomethyl-2-chlorobenzene

: 1352874-59-9
1-(6-bromo-pyridin-3-yl)-3-(2-chloro-benzyl)-1,3-dihydro-benzoimidazol-2-ylideneamine

Guidance literature:: With potassium iodide; In acetonitrile; at 110 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

: 69045-79-0
2-choro-5-iodopyridine

: 1352874-59-9
1-(6-bromo-pyridin-3-yl)-3-(2-chloro-benzyl)-1,3-dihydro-benzoimidazol-2-ylideneamine

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine / palladium diacetate / toluene / 48 h / Inert atmosphere; Reflux

2: tin(II) chloride dihdyrate / ethanol / 2 h / 70 °C

3: water; acetonitrile / 16 h / 20 °C

4: potassium iodide / acetonitrile / 0.17 h / 110 °C / Microwave irradiation

With tin(II) chloride dihdyrate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; potassium iodide; palladium diacetate; In ethanol; water; toluene; acetonitrile;

Reference yield:

: 88-74-4
2-nitro-aniline

: 1352874-59-9
1-(6-bromo-pyridin-3-yl)-3-(2-chloro-benzyl)-1,3-dihydro-benzoimidazol-2-ylideneamine

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine / palladium diacetate / toluene / 48 h / Inert atmosphere; Reflux

2: tin(II) chloride dihdyrate / ethanol / 2 h / 70 °C

3: water; acetonitrile / 16 h / 20 °C

4: potassium iodide / acetonitrile / 0.17 h / 110 °C / Microwave irradiation

With tin(II) chloride dihdyrate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; potassium iodide; palladium diacetate; In ethanol; water; toluene; acetonitrile;