5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole

Base Information

Chemical Name:5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole
CAS No.:1607830-08-9
Molecular Formula:C₂₇H₃₁NO₂SSi
Molecular Weight:461.7
Hs Code.:

Synonyms:5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole

Suppliers and Price of 5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole

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Technology Process of 5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole

There total 1 articles about 5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1607830-04-5
N-(7-(benzyldimethylsilyl)hepta-1,6-diyn-1-yl)-N-(3-bromobut-3-en-1-yl)-4-methylbenzenesulfonamide

: 1607830-08-9
5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In acetonitrile; at 80 ℃; for 16h; Concentration; Inert atmosphere; Sealed tube;
DOI:10.1039/c3cc45634j

Reference yield: 68.0%

: 101349-79-5
2-phenylvinyl iodide

: 1607830-08-9
5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole

: 1607830-11-4
(E)-5-styryl-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole

Guidance literature:: 2-phenylvinyl iodide; 5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.166667h; Inert atmosphere;

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver(l) oxide; In tetrahydrofuran; at 20 ℃; for 22h;
DOI:10.1039/c3cc45634j

Reference yield: 67.0%

: 101349-79-5
2-phenylvinyl iodide

: 1607830-08-9
5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole

: 1607830-12-5
1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole

Guidance literature:: 2-phenylvinyl iodide; 5-(benzyldimethylsilyl)-1-tosyl-1,2,3,6,7,8-hexahydrocyclopenta[g]indole; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.166667h; Inert atmosphere;

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver(l) oxide; In tetrahydrofuran; at 20 ℃; for 17h;
DOI:10.1039/c3cc45634j