(4R,5S)-benzyl 4-((2-(benzyloxy)-2-oxoethoxy)carbamoyl)-5-hydroxy-2,2-dimethylthiazolidine-3-carboxylate

Base Information

Chemical Name:(4R,5S)-benzyl 4-((2-(benzyloxy)-2-oxoethoxy)carbamoyl)-5-hydroxy-2,2-dimethylthiazolidine-3-carboxylate
CAS No.:1334521-66-2
Molecular Formula:C₂₃H₂₆N₂O₇S
Molecular Weight:474.535
Hs Code.:

Synonyms:(4R,5S)-benzyl 4-((2-(benzyloxy)-2-oxoethoxy)carbamoyl)-5-hydroxy-2,2-dimethylthiazolidine-3-carboxylate

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Chemical Property of (4R,5S)-benzyl 4-((2-(benzyloxy)-2-oxoethoxy)carbamoyl)-5-hydroxy-2,2-dimethylthiazolidine-3-carboxylate

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Technology Process of (4R,5S)-benzyl 4-((2-(benzyloxy)-2-oxoethoxy)carbamoyl)-5-hydroxy-2,2-dimethylthiazolidine-3-carboxylate

There total 5 articles about (4R,5S)-benzyl 4-((2-(benzyloxy)-2-oxoethoxy)carbamoyl)-5-hydroxy-2,2-dimethylthiazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₆N₂O₈S

: 1334521-66-2
(4R,5S)-benzyl 4-((2-(benzyloxy)-2-oxoethoxy)carbamoyl)-5-hydroxy-2,2-dimethylthiazolidine-3-carboxylate

Guidance literature:: With dimethylsulfide; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.tetlet.2011.07.085

Reference yield:

: 46230-31-3
benzyl 2-(aminooxy)acetate

: 1334521-66-2
(4R,5S)-benzyl 4-((2-(benzyloxy)-2-oxoethoxy)carbamoyl)-5-hydroxy-2,2-dimethylthiazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: -20 °C

2: oxygen / tetrahydrofuran / -10 - 0 °C / UV-irradiation

3: dimethylsulfide / tetrahydrofuran / 20 °C

With dimethylsulfide; oxygen; In tetrahydrofuran; 2: Pummerer type rearrangement;
DOI:10.1016/j.tetlet.2011.07.085

Reference yield:

: C₁₉H₂₅NO₆S

: 1334521-66-2
(4R,5S)-benzyl 4-((2-(benzyloxy)-2-oxoethoxy)carbamoyl)-5-hydroxy-2,2-dimethylthiazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: -20 °C

2: oxygen / tetrahydrofuran / -10 - 0 °C / UV-irradiation

3: dimethylsulfide / tetrahydrofuran / 20 °C

With dimethylsulfide; oxygen; In tetrahydrofuran; 2: Pummerer type rearrangement;
DOI:10.1016/j.tetlet.2011.07.085