digitoxigenin 3'',4''-di-O-tert-butyldiphenylsilyl-2'',6''-dideoxy-β-D-ribo-hexopyranosyl-(1->4)-3'-O-acetyl-2',6'-dideoxy-β-D-ribo-hexopyranoside

Base Information

Chemical Name:digitoxigenin 3'',4''-di-O-tert-butyldiphenylsilyl-2'',6''-dideoxy-β-D-ribo-hexopyranosyl-(1->4)-3'-O-acetyl-2',6'-dideoxy-β-D-ribo-hexopyranoside
CAS No.:1345697-44-0
Molecular Formula:C₆₉H₉₂O₁₁Si₂
Molecular Weight:1153.65
Hs Code.:

Synonyms:digitoxigenin 3'',4''-di-O-tert-butyldiphenylsilyl-2'',6''-dideoxy-β-D-ribo-hexopyranosyl-(1->4)-3'-O-acetyl-2',6'-dideoxy-β-D-ribo-hexopyranoside

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Chemical Property of digitoxigenin 3'',4''-di-O-tert-butyldiphenylsilyl-2'',6''-dideoxy-β-D-ribo-hexopyranosyl-(1->4)-3'-O-acetyl-2',6'-dideoxy-β-D-ribo-hexopyranoside

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Technology Process of digitoxigenin 3'',4''-di-O-tert-butyldiphenylsilyl-2'',6''-dideoxy-β-D-ribo-hexopyranosyl-(1->4)-3'-O-acetyl-2',6'-dideoxy-β-D-ribo-hexopyranoside

There total 1 articles about digitoxigenin 3'',4''-di-O-tert-butyldiphenylsilyl-2'',6''-dideoxy-β-D-ribo-hexopyranosyl-(1->4)-3'-O-acetyl-2',6'-dideoxy-β-D-ribo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 74264-36-1
digitoxigenin 3-O-acetyl-2,6-dideoxy-β-D-ribo-hexopyranoside

: 3,4-di-O-tert-butyldiphenylsilyl-2,6-dideoxy-D-ribo-hexopyranosyl o-cyclopropylethynylbenzoate

: 1345697-44-0
digitoxigenin 3'',4''-di-O-tert-butyldiphenylsilyl-2'',6''-dideoxy-β-D-ribo-hexopyranosyl-(1->4)-3'-O-acetyl-2',6'-dideoxy-β-D-ribo-hexopyranoside

Guidance literature:: With triphenylphosphinegold(I) triflate; In dichloromethane; toluene; at -40 ℃; for 2h; diastereoselective reaction; Molecular sieve;
DOI:10.1021/jo201850z