Technology Process of C25H36BrN3O4Si
There total 3 articles about C25H36BrN3O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate; Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
for 2.5h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / dichloromethane; hexane / 4 h / -78 °C
2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2.5 h / 20 °C
With
diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane;
In
hexane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C
1.2: 3 h / 20 °C
2.1: diisobutylaluminium hydride / dichloromethane; hexane / 4 h / -78 °C
3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2.5 h / 20 °C
With
sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane;
In
hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;