C₁₅H₈⁽²⁾H₅N

Base Information

• Chemical Name: C₁₅H₈⁽²⁾H₅N
• CAS No.: 877203-70-8
• Molecular Formula: C₁₅H₁₃N
• Molecular Weight: 212.235
• Mol file: 877203-70-8.mol

Synonyms:C₁₅H₈⁽²⁾H₅N

Chemical Property of C₁₅H₈⁽²⁾H₅N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₅H₈⁽²⁾H₅N

There total 5 articles about C₁₅H₈⁽²⁾H₅N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H10(2)H5NO → C15H8(2)H5N (877203-70-8)

Guidance literature:

With tributylphosphine; di-isopropyl azodicarboxylate; In acetonitrile; at 20 ℃; for 2h;

DOI:10.1021/ja058026j

Reference yield:

C15H9(2)H5 (877203-67-3) → C15H8(2)H5N (877203-70-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 0.168 g / mCPBA; NaHCO₃ / CH₂Cl₂ / 0 °C

2: 102 mg / BF₃*OEt₂ / diethyl ether / 0.02 h / 20 °C

3: NaOAc; NH₂OH*HCl / methanol; H₂O / 4 h / 20 °C

4: DIAD; tri-n-butylphosphine / acetonitrile / 2 h / 20 °C

With tributylphosphine; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; hydroxylamine hydrochloride; sodium acetate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; dichloromethane; water; acetonitrile;

DOI:10.1021/ja058026j

Reference yield:

C15H9(2)H5O (877203-68-4) → C15H8(2)H5N (877203-70-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 102 mg / BF₃*OEt₂ / diethyl ether / 0.02 h / 20 °C

2: NaOAc; NH₂OH*HCl / methanol; H₂O / 4 h / 20 °C

3: DIAD; tri-n-butylphosphine / acetonitrile / 2 h / 20 °C

With tributylphosphine; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; hydroxylamine hydrochloride; sodium acetate; In methanol; diethyl ether; water; acetonitrile;

DOI:10.1021/ja058026j

upstream raw materials:

C₁₅H₉⁽²⁾H₅

C₁₅H₉⁽²⁾H₅O

C₁₅H₉⁽²⁾H₅O

2,3,4,5,6-Pentadeuteriobenzophenon