dimethyl (3-cyclohexylideneprop-2-en-1-yl)[(2E)-penta-2,4-dien-1-yl]propanedioate

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Chemical Name:dimethyl (3-cyclohexylideneprop-2-en-1-yl)[(2E)-penta-2,4-dien-1-yl]propanedioate
CAS No.:1152437-72-3
Molecular Formula:C₁₉H₂₆O₄
Molecular Weight:318.413
Hs Code.:

Synonyms:dimethyl (3-cyclohexylideneprop-2-en-1-yl)[(2E)-penta-2,4-dien-1-yl]propanedioate

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Chemical Property of dimethyl (3-cyclohexylideneprop-2-en-1-yl)[(2E)-penta-2,4-dien-1-yl]propanedioate

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Technology Process of dimethyl (3-cyclohexylideneprop-2-en-1-yl)[(2E)-penta-2,4-dien-1-yl]propanedioate

There total 2 articles about dimethyl (3-cyclohexylideneprop-2-en-1-yl)[(2E)-penta-2,4-dien-1-yl]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 3-cyclohexylideneallyl methanesulfonate

: 75283-58-8
2-(2,4-pentadienyl)malonic acid dimethyl ester

: 1152437-72-3
dimethyl (3-cyclohexylideneprop-2-en-1-yl)[(2E)-penta-2,4-dien-1-yl]propanedioate

Guidance literature:: 2-(2,4-pentadienyl)malonic acid dimethyl ester; With sodium hydride; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

3-cyclohexylideneallyl methanesulfonate; In tetrahydrofuran; at 21 - 25 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja905415r

Reference yield: 59.0%

: 75283-58-8
2-(2,4-pentadienyl)malonic acid dimethyl ester

: 56037-79-7
3-cyclohexylideneprop-2-en-1-ol

: 1152437-72-3
dimethyl (3-cyclohexylideneprop-2-en-1-yl)[(2E)-penta-2,4-dien-1-yl]propanedioate

Guidance literature:: 2-(2,4-pentadienyl)malonic acid dimethyl ester; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

3-cyclohexylideneprop-2-en-1-ol; With sodium iodide; In tetrahydrofuran; dimethyl sulfoxide; at 0 - 20 ℃; Inert atmosphere;

Reference yield: 91.0%

: 1152437-72-3
dimethyl (3-cyclohexylideneprop-2-en-1-yl)[(2E)-penta-2,4-dien-1-yl]propanedioate

: dimethyl 7-cyclohexylidene-3,3a,7,7a-tetrahydro-1H-indene-2,2(6H)-dicarboxylate

Guidance literature:: With silver hexafluoroantimonate; tris(2,4-di-tert-butylphenyl)phosphite gold(I) chloride; In dichloromethane; at 0 ℃; for 1h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ja905415r