(2S,2'S)-diethyl 2,2'-(6-nitro-6-phenyl-1,4-diazepane-1,4-diyl)dipropanoate

Base Information

Chemical Name:(2S,2'S)-diethyl 2,2'-(6-nitro-6-phenyl-1,4-diazepane-1,4-diyl)dipropanoate
CAS No.:1416732-12-1
Molecular Formula:C₂₁H₃₁N₃O₆
Molecular Weight:421.494
Hs Code.:

Synonyms:(2S,2'S)-diethyl 2,2'-(6-nitro-6-phenyl-1,4-diazepane-1,4-diyl)dipropanoate

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Chemical Property of (2S,2'S)-diethyl 2,2'-(6-nitro-6-phenyl-1,4-diazepane-1,4-diyl)dipropanoate

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Technology Process of (2S,2'S)-diethyl 2,2'-(6-nitro-6-phenyl-1,4-diazepane-1,4-diyl)dipropanoate

There total 2 articles about (2S,2'S)-diethyl 2,2'-(6-nitro-6-phenyl-1,4-diazepane-1,4-diyl)dipropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1416732-08-5
6-nitro-6-phenyl-1,4-diazepane

: 84028-89-7
ethyl (R)-2-trifluoromethylsulfonyloxypropanoate

: 1416732-12-1
(2S,2'S)-diethyl 2,2'-(6-nitro-6-phenyl-1,4-diazepane-1,4-diyl)dipropanoate

Guidance literature:: With potassium carbonate; In acetonitrile; at 34.84 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2cc37544c

Reference yield:

: 1416732-07-4
1,4-bis(2,4-dimethoxybenzyl)-6-nitro-6-phenyl-1,4-diazepane

: 1416732-12-1
(2S,2'S)-diethyl 2,2'-(6-nitro-6-phenyl-1,4-diazepane-1,4-diyl)dipropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

2: potassium carbonate / acetonitrile / 24 h / 34.84 °C / Inert atmosphere

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1039/c2cc37544c

Reference yield:

: 1416732-12-1
(2S,2'S)-diethyl 2,2'-(6-nitro-6-phenyl-1,4-diazepane-1,4-diyl)dipropanoate

: 1416732-14-3
(2S,2'S)-diethyl 2,2'-(6-((S)-1-ethoxy-1-oxopropan-2-ylamino)-6-phenyl-1,4-diazepane-1,4-diyl)dipropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / ethanol; methanol / 3 h / 24.84 °C / Inert atmosphere

2: potassium carbonate / acetonitrile / 18 h / 34.84 °C / Inert atmosphere

With hydrogen; potassium carbonate; In methanol; ethanol; acetonitrile;
DOI:10.1039/c2cc37544c