C₃₆H₆₂SiO₄

Base Information

Chemical Name:C₃₆H₆₂SiO₄
CAS No.:947769-28-0
Molecular Formula:C₃₆H₆₂O₄Si
Molecular Weight:586.971
Hs Code.:

C<sub>36</sub>H<sub>62</sub>SiO<sub>4</sub>

Synonyms:C₃₆H₆₂SiO₄

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Chemical Property of C₃₆H₆₂SiO₄

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Technology Process of C₃₆H₆₂SiO₄

There total 11 articles about C₃₆H₆₂SiO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 947769-26-8
C₃₈H₆₄SSiO₄H₂

: 947769-28-0
C₃₆H₆₂SiO₄

Guidance literature:: With water; sodium hydrogencarbonate; methyl iodide; In acetone; at 45 ℃; for 14h;
DOI:10.1021/ol071024e

Reference yield:

: C₁₈H₃₅ISiO

: 947769-28-0
C₃₆H₆₂SiO₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: 92 percent / Pd(PPh₃)4 / tetrahydrofuran / 14 h / 0 °C

2.1: DIBAL-H / CH₂Cl₂ / 3 h / -78 °C

3.1: 99 percent / CBr₄; 2,6-lutidine; PPh₃ / CH₂Cl₂ / 20 °C

4.1: t-BuLi / diethyl ether; pentane / 0.33 h / -78 - -40 °C

4.2: 72 mg / diethyl ether; pentane / 0.33 h / -78 °C

5.1: 87 percent / LiI; LiAlH₄ / diethyl ether / 0.33 h / -100 °C

6.1: 70 percent / MeI; NaHCO₃; H₂O / acetone / 14 h / 45 °C

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; carbon tetrabromide; water; tert.-butyl lithium; diisobutylaluminium hydride; sodium hydrogencarbonate; triphenylphosphine; lithium iodide; methyl iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; pentane;
DOI:10.1021/ol071024e

Reference yield:

: 947769-16-6
C₂₂H₄₄SiO₂

: 947769-28-0
C₃₆H₆₂SiO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: 99 percent / CBr₄; 2,6-lutidine; PPh₃ / CH₂Cl₂ / 20 °C

2.1: t-BuLi / diethyl ether; pentane / 0.33 h / -78 - -40 °C

2.2: 72 mg / diethyl ether; pentane / 0.33 h / -78 °C

3.1: 87 percent / LiI; LiAlH₄ / diethyl ether / 0.33 h / -100 °C

4.1: 70 percent / MeI; NaHCO₃; H₂O / acetone / 14 h / 45 °C

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; carbon tetrabromide; water; tert.-butyl lithium; sodium hydrogencarbonate; triphenylphosphine; lithium iodide; methyl iodide; In diethyl ether; dichloromethane; acetone; pentane;
DOI:10.1021/ol071024e