Technology Process of C37H54N6O11
There total 7 articles about C37H54N6O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine tris(hydrogen fluoride);
In
acetonitrile;
at 50 ℃;
for 24h;
Inert atmosphere;
DOI:10.1021/jo500039d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere
2: triethylphosphine / tetrahydrofuran; toluene / 30 h / 20 °C / Inert atmosphere
3: toluene / 48 h / 70 °C / Inert atmosphere
4: triethylamine tris(hydrogen fluoride) / acetonitrile / 24 h / 50 °C / Inert atmosphere
With
sulfur trioxide pyridine complex; triethylamine tris(hydrogen fluoride); triethylamine; triethylphosphine;
In
tetrahydrofuran; dimethyl sulfoxide; toluene; acetonitrile;
2: |Staudinger Azide Reduction / 3: |Ugi Condensation;
DOI:10.1021/jo500039d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
2: toluene / 48 h / 70 °C / Inert atmosphere
3: triethylamine tris(hydrogen fluoride) / acetonitrile / 24 h / 50 °C / Inert atmosphere
With
sodium hydrogencarbonate; triethylamine tris(hydrogen fluoride);
In
N,N-dimethyl-formamide; toluene; acetonitrile;
2: |Ugi Condensation;
DOI:10.1021/jo500039d