6,6-dithiobis(2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl dibenzyl phosphate)

Base Information

• Chemical Name: 6,6-dithiobis(2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl dibenzyl phosphate)
• CAS No.: 125164-15-0
• Molecular Formula: C₈₂H₈₄O₁₆P₂S₂
• Molecular Weight: 1451.64
• Mol file: 125164-15-0.mol

Synonyms:6,6-dithiobis(2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl dibenzyl phosphate)

Chemical Property of 6,6-dithiobis(2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl dibenzyl phosphate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 6,6-dithiobis(2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl dibenzyl phosphate)

There total 1 articles about 6,6-dithiobis(2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2,3,4-tri-O-benzyl-6-O-trifluoromethanesulfonyl-α-D-glucopyranosyl dibenzyl phosphate → 6,6-dithiobis(2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl dibenzyl phosphate) (125164-15-0)

Guidance literature:

With t-Bu₄NHSO₃; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1016/0008-6215(89)85043-8

Reference yield: 74.0%

6,6-dithiobis(2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl dibenzyl phosphate) (125164-15-0) → 2,3,4-tri-O-benzyl-6-deoxy-6-sulfo-α-D-glucopyranosyl dibenzyl phosphate sodium salt

Guidance literature:

With sodium acetate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1.) 0 deg C, 1 h, 2.) RT; 1 h,;

DOI:10.1016/0008-6215(89)85043-8