3,6,7,10,11-pentakis(hexyloxy)triphenylen-2-yl 1,1,1-trifluoromethanesulfonate

Base Information

Chemical Name:3,6,7,10,11-pentakis(hexyloxy)triphenylen-2-yl 1,1,1-trifluoromethanesulfonate
CAS No.:1244773-43-0
Molecular Formula:C₄₉H₇₁F₃O₈S
Molecular Weight:877.159
Hs Code.:

Synonyms:3,6,7,10,11-pentakis(hexyloxy)triphenylen-2-yl 1,1,1-trifluoromethanesulfonate

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Chemical Property of 3,6,7,10,11-pentakis(hexyloxy)triphenylen-2-yl 1,1,1-trifluoromethanesulfonate

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Technology Process of 3,6,7,10,11-pentakis(hexyloxy)triphenylen-2-yl 1,1,1-trifluoromethanesulfonate

There total 1 articles about 3,6,7,10,11-pentakis(hexyloxy)triphenylen-2-yl 1,1,1-trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 70351-86-9
2,3,6,7,10,11-hexakis(hexyloxy)triphenylene

: 1244773-43-0
3,6,7,10,11-pentakis(hexyloxy)triphenylen-2-yl 1,1,1-trifluoromethanesulfonate

Guidance literature:: 2,3,6,7,10,11-hexakis(hexyloxy)triphenylene; With 2-bromo-1,3,2-benzodioxaborole; In dichloromethane; at 0 - 20 ℃;

trifluoromethylsulfonic anhydride; With pyridine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/hlca.201000333

Reference yield: 94.0%

: 80460-73-7
(4-aminophenyl)boronic acid hydrochloride

: 1244773-43-0
3,6,7,10,11-pentakis(hexyloxy)triphenylen-2-yl 1,1,1-trifluoromethanesulfonate

: C₅₄H₇₇NO₅

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 70 ℃; for 24h; Inert atmosphere;

Reference yield: 93.6%

: 1244773-43-0
3,6,7,10,11-pentakis(hexyloxy)triphenylen-2-yl 1,1,1-trifluoromethanesulfonate

: 121219-12-3
(4-pentylphenyl)boronic acid

: C₅₉H₈₆O₅

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1002/ejoc.201600270