3-(2-acetoxyethyl)-4-ethyl-2-tosylpyrrole

Base Information

Chemical Name:3-(2-acetoxyethyl)-4-ethyl-2-tosylpyrrole
CAS No.:917895-04-6
Molecular Formula:C₁₇H₂₁NO₄S
Molecular Weight:335.424
Hs Code.:

Synonyms:3-(2-acetoxyethyl)-4-ethyl-2-tosylpyrrole

Suppliers and Price of 3-(2-acetoxyethyl)-4-ethyl-2-tosylpyrrole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(2-acetoxyethyl)-4-ethyl-2-tosylpyrrole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(2-acetoxyethyl)-4-ethyl-2-tosylpyrrole

There total 3 articles about 3-(2-acetoxyethyl)-4-ethyl-2-tosylpyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 917895-03-5
4-nitrohexane-1,3-diyl diacetate

: 38622-91-2,36635-61-7
[(p-methylphenyl)sulfonylmethyl]isonitrile

: 917895-04-6
3-(2-acetoxyethyl)-4-ethyl-2-tosylpyrrole

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 5h;
DOI:10.1246/bcsj.79.1561

Reference yield:

: 917895-10-4
acetic acid 3-hydroxy-4-nitro-hexyl ester

: 917895-04-6
3-(2-acetoxyethyl)-4-ethyl-2-tosylpyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 2.28 g / 4-(dimethylamino)pyridine / tetrahydrofuran / 2 h / 20 °C

2: 59 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 5 h / 20 °C

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; acetonitrile; 2: Barton's method;
DOI:10.1246/bcsj.79.1561

Reference yield:

: 18545-28-3
3-acetoxypropanal

: 917895-04-6
3-(2-acetoxyethyl)-4-ethyl-2-tosylpyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / methanol / 2 h / 20 °C

2: 2.28 g / 4-(dimethylamino)pyridine / tetrahydrofuran / 2 h / 20 °C

3: 59 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 5 h / 20 °C

With dmap; potassium hydroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; acetonitrile; 1: Henry reaction / 3: Barton's method;
DOI:10.1246/bcsj.79.1561