(4E,8E,2S)-1-tert-butyldiphenylsilyloxy-4,8-diethyl-2-methyldecene-4,8-diene

Base Information

Chemical Name:(4E,8E,2S)-1-tert-butyldiphenylsilyloxy-4,8-diethyl-2-methyldecene-4,8-diene
CAS No.:1243715-47-0
Molecular Formula:C₃₁H₄₆OSi
Molecular Weight:462.791
Hs Code.:

Synonyms:(4E,8E,2S)-1-tert-butyldiphenylsilyloxy-4,8-diethyl-2-methyldecene-4,8-diene

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Chemical Property of (4E,8E,2S)-1-tert-butyldiphenylsilyloxy-4,8-diethyl-2-methyldecene-4,8-diene

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Technology Process of (4E,8E,2S)-1-tert-butyldiphenylsilyloxy-4,8-diethyl-2-methyldecene-4,8-diene

There total 1 articles about (4E,8E,2S)-1-tert-butyldiphenylsilyloxy-4,8-diethyl-2-methyldecene-4,8-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1009090-09-8
C₁₁H₁₉I

: 123444-67-7
(R)-3-[(tert-butyl)diphenylsilyloxy]-1-iodo-2-methylpropane

: 1243715-47-0
(4E,8E,2S)-1-tert-butyldiphenylsilyloxy-4,8-diethyl-2-methyldecene-4,8-diene

Guidance literature:: (R)-3-[(tert-butyl)diphenylsilyloxy]-1-iodo-2-methylpropane; With tert.-butyl lithium; zinc(II) chloride; In tetrahydrofuran; pentane; at -78 - 20 ℃;

C₁₁H₁₉I; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; pentane; at 20 ℃; for 16h; Darkness;
DOI:10.1021/ol100541e

Reference yield: 57.0%

: 1243715-47-0
(4E,8E,2S)-1-tert-butyldiphenylsilyloxy-4,8-diethyl-2-methyldecene-4,8-diene

: (2S)-1-tert-butyldiphenylsiloxy-4,8-diethyl-2-methyl-4,5;8,9-diepoxydecane

: 1243716-23-5
(2S,4R,5R,8R,9R)-1-tert-butyldiphenylsiloxy-4,8-diethyl-2-methyl-4,5;8,9-diepoxydecane

Guidance literature:: With Oxone; Shi's ketone; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In 1,2-dimethoxyethane; water; acetonitrile; at 0 ℃; for 2h; aq. buffer;
DOI:10.1021/ol100541e