2-(4-bromo-3-methyl-phenyl)-5-thioxo-5,6-dihydro-4H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7-one

Base Information

Chemical Name:2-(4-bromo-3-methyl-phenyl)-5-thioxo-5,6-dihydro-4H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7-one
CAS No.:1456613-90-3
Molecular Formula:C₁₁H₈BrN₅OS
Molecular Weight:338.187
Hs Code.:

Synonyms:2-(4-bromo-3-methyl-phenyl)-5-thioxo-5,6-dihydro-4H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7-one

Suppliers and Price of 2-(4-bromo-3-methyl-phenyl)-5-thioxo-5,6-dihydro-4H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(4-bromo-3-methyl-phenyl)-5-thioxo-5,6-dihydro-4H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7-one

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(4-bromo-3-methyl-phenyl)-5-thioxo-5,6-dihydro-4H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7-one

There total 5 articles about 2-(4-bromo-3-methyl-phenyl)-5-thioxo-5,6-dihydro-4H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1456614-12-2
C₁₃H₁₄BrN₅O₂S

: 1456613-90-3
2-(4-bromo-3-methyl-phenyl)-5-thioxo-5,6-dihydro-4H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7-one

Guidance literature:: With sodium hydroxide; In ethanol; water; at 100 ℃; for 0.333333h;
DOI:10.1016/j.ejmech.2013.06.051

Reference yield:

: C₉H₉BrN₄

: 1456613-90-3
2-(4-bromo-3-methyl-phenyl)-5-thioxo-5,6-dihydro-4H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7-one

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 20 °C

2: sodium hydroxide / ethanol; water / 0.33 h / 100 °C

With sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1111/cbdd.12171

Reference yield:

: C₉H₁₁BrN₄O

: 1456613-90-3
2-(4-bromo-3-methyl-phenyl)-5-thioxo-5,6-dihydro-4H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7-one

Guidance literature:: Multi-step reaction with 3 steps

1: water / 180 °C / Microwave irradiation

2: N,N-dimethyl-formamide / 5 h / 20 °C

3: sodium hydroxide / ethanol; water / 0.33 h / 100 °C

With sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.06.051