(2R,3S,4S)-2<(1R)-1-Hydroxyethyl>-1-<(1S)-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>-3,4-pyrrolidindiol

Base Information

Chemical Name:(2R,3S,4S)-2<(1R)-1-Hydroxyethyl>-1-<(1S)-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>-3,4-pyrrolidindiol
CAS No.:92898-55-0
Molecular Formula:C₁₃H₂₃NO₇
Molecular Weight:305.328
Hs Code.:

Synonyms:(2R,3S,4S)-2<(1R)-1-Hydroxyethyl>-1-<(1S)-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>-3,4-pyrrolidindiol

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Chemical Property of (2R,3S,4S)-2<(1R)-1-Hydroxyethyl>-1-<(1S)-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>-3,4-pyrrolidindiol

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Technology Process of (2R,3S,4S)-2<(1R)-1-Hydroxyethyl>-1-<(1S)-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>-3,4-pyrrolidindiol

There total 2 articles about (2R,3S,4S)-2<(1R)-1-Hydroxyethyl>-1-<(1S)-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>-3,4-pyrrolidindiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 92621-73-3
(1R,2S,3R,4aS,7R,8S,8aS,9aR)1,2,3,4a,7,8,8a,9a-Octahydro-1,2,7,8-tetrahydroxy-3-<(R)-1-hydroxyethyl>-6-hydroxymethylpyrrolo<2,1-b>benzoxazol

: 92898-55-0
(2R,3S,4S)-2<(1R)-1-Hydroxyethyl>-1-<(1S)-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>-3,4-pyrrolidindiol

Guidance literature:: With sodium tetrahydroborate; In water; for 76h; Ambient temperature;
DOI:10.1016/0008-6215(84)85333-1

Reference yield:

: 56180-94-0,68107-33-5,106864-09-9
acarbose

: 92898-55-0
(2R,3S,4S)-2<(1R)-1-Hydroxyethyl>-1-<(1S)-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>-3,4-pyrrolidindiol

Guidance literature:: Multi-step reaction with 2 steps

1: 2.8 g / 1M H₂SO₄ / 5 h / 130 °C

2: 92 percent / NaBH₄ / H₂O / 76 h / Ambient temperature

With sodium tetrahydroborate; sulfuric acid; In water;
DOI:10.1016/0008-6215(84)85333-1

Reference yield:

: 92898-55-0
(2R,3S,4S)-2<(1R)-1-Hydroxyethyl>-1-<(1S)-(1,4,6/5)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>-3,4-pyrrolidindiol

: 92691-71-9,678142-34-2,749145-39-9,778561-25-4
(2R,3S,4S)-2-<(1R)-1-Hydroxyethyl>pyrrolidin-3,4-diol

: 92567-51-6
(2R,3S,4S)-2-<(1R)-1-Hydroxyethyl>-1-<(1S)-(1,2,4/3)-2,3,4-trihydroxy-1-cyclohexanylmethyl>pyrrolidin-3,4-diol

Guidance literature:: With hydrogen; platinum(IV) oxide; In water; for 7h; under 2625.2 Torr; Ambient temperature;
DOI:10.1016/0008-6215(84)85333-1