2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>benzoic acid 3-hydroxypropyl ester

Base Information

Chemical Name:2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>benzoic acid 3-hydroxypropyl ester
CAS No.:147355-10-0
Molecular Formula:C₁₉H₂₈N₆O₃
Molecular Weight:388.47
Hs Code.:

Synonyms:2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>benzoic acid 3-hydroxypropyl ester

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Chemical Property of 2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>benzoic acid 3-hydroxypropyl ester

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Technology Process of 2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>benzoic acid 3-hydroxypropyl ester

There total 4 articles about 2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>benzoic acid 3-hydroxypropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 147355-10-0
2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>benzoic acid 3-hydroxypropyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 32 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / diethyl ether; tetrahydrofuran / 12 h / Ambient temperature

2: diisopropylethylamine / tetrahydrofuran / 1 h / 0 °C

3: NH₃ gas / tetrahydrofuran / 1 h / 0 °C

4: diisopropylamine / tetrahydrofuran / 4 h / Heating

With dmap; ammonia; diisopropylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00056a014

Reference yield:

: anthranilic acid hydroxypropyl ester

: 147355-10-0
2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>benzoic acid 3-hydroxypropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diisopropylethylamine / tetrahydrofuran / 1 h / 0 °C

2: NH₃ gas / tetrahydrofuran / 1 h / 0 °C

3: diisopropylamine / tetrahydrofuran / 4 h / Heating

With ammonia; diisopropylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;
DOI:10.1021/ja00056a014

Reference yield:

: 2-(4,6-Dichloro-[1,3,5]triazin-2-ylamino)-benzoic acid 3-hydroxy-propyl ester

: 147355-10-0
2-<<4-amino-6-<(3,3-dimethylbutyl)amino>-1,3,5-triazin-2-yl>amino>benzoic acid 3-hydroxypropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ gas / tetrahydrofuran / 1 h / 0 °C

2: diisopropylamine / tetrahydrofuran / 4 h / Heating

With ammonia; diisopropylamine; In tetrahydrofuran;
DOI:10.1021/ja00056a014