C₃₅H₄₈N₆O₉

Base Information

Chemical Name:C₃₅H₄₈N₆O₉
CAS No.:1360566-57-9
Molecular Formula:C₃₅H₄₈N₆O₉
Molecular Weight:696.801
Hs Code.:

C<sub>35</sub>H<sub>48</sub>N<sub>6</sub>O<sub>9</sub>

Synonyms:C₃₅H₄₈N₆O₉

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Chemical Property of C₃₅H₄₈N₆O₉

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Technology Process of C₃₅H₄₈N₆O₉

There total 11 articles about C₃₅H₄₈N₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1360566-56-8
C₄₃H₅₄N₆O₁₁

: 1360566-57-9
C₃₅H₄₈N₆O₉

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; at 0 ℃; for 5h; Inert atmosphere;
DOI:10.1002/chem.201101058

Reference yield:

: 1360566-51-3
C₂₄H₄₀N₂O₆Si

: 1360566-57-9
C₃₅H₄₈N₆O₉

Guidance literature:: Multi-step reaction with 9 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / -40 °C

1.2: 5 h / -40 - 0 °C

2.1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C

3.1: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere

4.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

5.1: monochloromethanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

7.1: 20 % Pd(OH)2/C; hydrogen / methanol / 3 h / 20 °C

8.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 2 h / 20 °C

9.1: sodium methylate / tetrahydrofuran; methanol / 5 h / 0 °C / Inert atmosphere

With hydrogenchloride; titanium(III) chloride; monochloromethanesulfonyl chloride; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; sodium methylate; sodium acetate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101058

Reference yield:

: 1221741-69-0
C₂₄H₄₂N₂O₅Si

: 1360566-57-9
C₃₅H₄₈N₆O₉

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C

2: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere

3: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

4: monochloromethanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

6: 20 % Pd(OH)2/C; hydrogen / methanol / 3 h / 20 °C

7: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 2 h / 20 °C

8: sodium methylate / tetrahydrofuran; methanol / 5 h / 0 °C / Inert atmosphere

With hydrogenchloride; titanium(III) chloride; monochloromethanesulfonyl chloride; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; sodium methylate; sodium acetate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101058