1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2',3',4'-tri-O-acetyl-α-L-rhamnopyranosyl)-α-D-glucopyranose

Base Information

Chemical Name:1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2',3',4'-tri-O-acetyl-α-L-rhamnopyranosyl)-α-D-glucopyranose
CAS No.:86158-29-4
Molecular Formula:C₃₁H₃₈O₁₇
Molecular Weight:682.633
Hs Code.:

Synonyms:1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2',3',4'-tri-O-acetyl-α-L-rhamnopyranosyl)-α-D-glucopyranose

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Chemical Property of 1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2',3',4'-tri-O-acetyl-α-L-rhamnopyranosyl)-α-D-glucopyranose

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Technology Process of 1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2',3',4'-tri-O-acetyl-α-L-rhamnopyranosyl)-α-D-glucopyranose

There total 4 articles about 1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2',3',4'-tri-O-acetyl-α-L-rhamnopyranosyl)-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28642-64-0
methyl 4,6-O-benzylidene-2-O-benzoyl-α-D-glucopyranoside

: 86158-29-4
1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2',3',4'-tri-O-acetyl-α-L-rhamnopyranosyl)-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 62.3 percent / silver triflate, 1,1,3,3-tetramethylurea / CH₂Cl₂ / 4 h / Ambient temperature

2: 60percent AcOH / 0.5 h / 100 °C

3: pyridine / 48 h / Ambient temperature

4: 52.1 percent / H₂SO₄ / 4 h / Ambient temperature

With pyridine; sulfuric acid; silver trifluoromethanesulfonate; acetic acid; tetramethylurea; In dichloromethane;

Reference yield:

: 5160-09-8
2,3,4‐tri‐O‐acetyl-α-L‐rhamnopyranosyl chloride

: 86158-29-4
1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2',3',4'-tri-O-acetyl-α-L-rhamnopyranosyl)-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 62.3 percent / silver triflate, 1,1,3,3-tetramethylurea / CH₂Cl₂ / 4 h / Ambient temperature

2: 60percent AcOH / 0.5 h / 100 °C

3: pyridine / 48 h / Ambient temperature

4: 52.1 percent / H₂SO₄ / 4 h / Ambient temperature

With pyridine; sulfuric acid; silver trifluoromethanesulfonate; acetic acid; tetramethylurea; In dichloromethane;

Reference yield:

: 221002-64-8
methyl 2,3,4-tri-O-acetyl-O-α-L-rhamnopyranosyl-(1->3)-2-O-benzoyI-O-α-D-glucopyranoside

: 86158-29-4
1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2',3',4'-tri-O-acetyl-α-L-rhamnopyranosyl)-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 48 h / Ambient temperature

2: 52.1 percent / H₂SO₄ / 4 h / Ambient temperature

With pyridine; sulfuric acid;