5'-N-(N-benzyloxycarbonyl-L-phenylalanyl)-5'-amino-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine

Base Information

Chemical Name:5'-N-(N-benzyloxycarbonyl-L-phenylalanyl)-5'-amino-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine
CAS No.:84045-04-5
Molecular Formula:C₂₉H₃₄N₄O₈
Molecular Weight:566.611
Hs Code.:

Synonyms:5'-N-(N-benzyloxycarbonyl-L-phenylalanyl)-5'-amino-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine

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Chemical Property of 5'-N-(N-benzyloxycarbonyl-L-phenylalanyl)-5'-amino-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine

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Technology Process of 5'-N-(N-benzyloxycarbonyl-L-phenylalanyl)-5'-amino-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine

There total 4 articles about 5'-N-(N-benzyloxycarbonyl-L-phenylalanyl)-5'-amino-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.7%

: 2578-84-9
N-benzyloxycarbonyl-L-phenylalanine p-nitrophenyl ester

: 84045-01-2
5'-amino-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine

: 84045-04-5
5'-N-(N-benzyloxycarbonyl-L-phenylalanyl)-5'-amino-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine

Guidance literature:: In tetrahydrofuran; for 48h; Ambient temperature;

Reference yield:

: 84045-00-1
5'-azido-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine

: 84045-04-5
5'-N-(N-benzyloxycarbonyl-L-phenylalanyl)-5'-amino-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine

Guidance literature:: Multi-step reaction with 2 steps

1: 455 mg / H₂ / Pd-black / ethanol / 5 h / 2625.2 Torr

2: 56.7 percent / tetrahydrofuran / 48 h / Ambient temperature

With hydrogen; palladium; In tetrahydrofuran; ethanol;

Reference yield:

: 84044-99-5
2',3'-O-isopropylidene-5'-O-methylsulphonyl-5,6-dihydrouridine

: 84045-04-5
5'-N-(N-benzyloxycarbonyl-L-phenylalanyl)-5'-amino-5'-deoxy-2',3'-O-isopropylidene-5,6-dihydrouridine

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / NaN₃ / dimethylformamide / 7 h / 85 °C

2: 455 mg / H₂ / Pd-black / ethanol / 5 h / 2625.2 Torr

3: 56.7 percent / tetrahydrofuran / 48 h / Ambient temperature

With sodium azide; hydrogen; palladium; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;