2-(benzyloxycarbonylamino)-2-deoxy-3,4:5,6-di-O-isopropylidene-aldehydo-D-glucose dibenzyl acetal

Base Information

• Chemical Name: 2-(benzyloxycarbonylamino)-2-deoxy-3,4:5,6-di-O-isopropylidene-aldehydo-D-glucose dibenzyl acetal
• CAS No.: 73707-69-4
• Molecular Formula: C₃₄H₄₁NO₈
• Molecular Weight: 591.701

Synonyms:2-(benzyloxycarbonylamino)-2-deoxy-3,4:5,6-di-O-isopropylidene-aldehydo-D-glucose dibenzyl acetal

Chemical Property of 2-(benzyloxycarbonylamino)-2-deoxy-3,4:5,6-di-O-isopropylidene-aldehydo-D-glucose dibenzyl acetal

Chemical Property:

Purity/Quality:

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Technology Process of 2-(benzyloxycarbonylamino)-2-deoxy-3,4:5,6-di-O-isopropylidene-aldehydo-D-glucose dibenzyl acetal

There total 2 articles about 2-(benzyloxycarbonylamino)-2-deoxy-3,4:5,6-di-O-isopropylidene-aldehydo-D-glucose dibenzyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

2-carbobenzyloxyamino-2-deoxy-D-glucopyranose (3006-58-4,13030-01-8,42890-10-8,42973-23-9,77059-32-6,121785-09-9,7474-40-0) + 2,2-dibenzyloxypropane (58886-34-3) → 2-(benzyloxycarbonylamino)-2-deoxy-3,4:5,6-di-O-isopropylidene-aldehydo-D-glucose dibenzyl acetal (73707-69-4)

Guidance literature:

With toluene-4-sulfonic acid; In 1,4-dioxane; at 65 ℃; for 2h;

DOI:10.1016/S0008-6215(00)83838-0

Reference yield:

2-carbobenzyloxyamino-2-deoxy-D-glucopyranose (3006-58-4,13030-01-8,42890-10-8,42973-23-9,77059-32-6,121785-09-9,7474-40-0) + 2,2-dibenzyloxypropane (58886-34-3) → [(R)-2,2-Bis-benzyloxy-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-carbamic acid benzyl ester (73707-69-4)

Guidance literature:

toluene-4-sulfonic acid; at 65 ℃; for 2h;

DOI:10.1016/0008-6215(84)85110-1

upstream raw materials:

2-carbobenzyloxyamino-2-deoxy-D-glucopyranose

2,2-dibenzyloxypropane

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