6-phenyl-2,3-dihydro-1H-benzo[b]cyclopenta[3,4]pyrazolo[5,1-f][1,6]naphthyridine

Base Information

Chemical Name:6-phenyl-2,3-dihydro-1H-benzo[b]cyclopenta[3,4]pyrazolo[5,1-f][1,6]naphthyridine
CAS No.:1428586-62-2
Molecular Formula:C₂₃H₁₇N₃
Molecular Weight:335.408
Hs Code.:

Synonyms:6-phenyl-2,3-dihydro-1H-benzo[b]cyclopenta[3,4]pyrazolo[5,1-f][1,6]naphthyridine

Suppliers and Price of 6-phenyl-2,3-dihydro-1H-benzo[b]cyclopenta[3,4]pyrazolo[5,1-f][1,6]naphthyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-phenyl-2,3-dihydro-1H-benzo[b]cyclopenta[3,4]pyrazolo[5,1-f][1,6]naphthyridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-phenyl-2,3-dihydro-1H-benzo[b]cyclopenta[3,4]pyrazolo[5,1-f][1,6]naphthyridine

There total 5 articles about 6-phenyl-2,3-dihydro-1H-benzo[b]cyclopenta[3,4]pyrazolo[5,1-f][1,6]naphthyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₁₉N₃O₂S

: 120-92-3
cyclopentanone

: 1428586-62-2
6-phenyl-2,3-dihydro-1H-benzo[b]cyclopenta[3,4]pyrazolo[5,1-f][1,6]naphthyridine

Guidance literature:: With potassium phosphate; In ethanol; at 70 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2013.02.060

Reference yield:

: 868765-12-2
2-phenylethynyl-quinoline-3-carbaldehyde

: 1428586-62-2
6-phenyl-2,3-dihydro-1H-benzo[b]cyclopenta[3,4]pyrazolo[5,1-f][1,6]naphthyridine

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 0.17 h / 20 °C / Inert atmosphere

2: silver trifluoromethanesulfonate / ethanol / 70 °C / Inert atmosphere

3: potassium phosphate / ethanol / 70 °C / Inert atmosphere

With potassium phosphate; silver trifluoromethanesulfonate; In ethanol;
DOI:10.1016/j.tet.2013.02.060

Reference yield:

: 73568-25-9
2-chloro-3-quinoline carboxaldehyde

: 1428586-62-2
6-phenyl-2,3-dihydro-1H-benzo[b]cyclopenta[3,4]pyrazolo[5,1-f][1,6]naphthyridine

Guidance literature:: Multi-step reaction with 4 steps

1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; triethylamine / acetonitrile / 80 °C / Inert atmosphere

2: ethanol / 0.17 h / 20 °C / Inert atmosphere

3: silver trifluoromethanesulfonate / ethanol / 70 °C / Inert atmosphere

4: potassium phosphate / ethanol / 70 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; silver trifluoromethanesulfonate; triethylamine; triphenylphosphine; In ethanol; acetonitrile; 1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.tet.2013.02.060