Technology Process of C66H87N11O2
There total 7 articles about C66H87N11O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
ethanol; water; toluene;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1002/chem.201304161
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(ll) sulfate pentahydrate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; sodium L-ascorbate / toluene; water; ethanol / 12 h / 20 °C / Inert atmosphere
2: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
3: potassium fluoride / methanol; tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
4: copper(ll) sulfate pentahydrate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; sodium L-ascorbate / toluene; water; ethanol / 12 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; potassium fluoride; copper(l) iodide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; triethylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
tetrahydrofuran; methanol; ethanol; water; toluene;
DOI:10.1002/chem.201304161
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 15 h / 20 °C / Inert atmosphere
2: copper(ll) sulfate pentahydrate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; sodium L-ascorbate / toluene; water; ethanol / 12 h / 20 °C / Inert atmosphere
3: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
4: potassium fluoride / methanol; tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
5: copper(ll) sulfate pentahydrate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; sodium L-ascorbate / toluene; water; ethanol / 12 h / 20 °C / Inert atmosphere
With
dmap; bis-triphenylphosphine-palladium(II) chloride; potassium fluoride; copper(l) iodide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene;
DOI:10.1002/chem.201304161