propane-2-sulfonic acid (7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoyl)-amide

Base Information

Chemical Name:propane-2-sulfonic acid (7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoyl)-amide
CAS No.:1026682-12-1
Molecular Formula:C₄₃H₈₃NO₆S₂Si₃
Molecular Weight:858.524
Hs Code.:

propane-2-sulfonic acid (7-{3,5-bis-(<i>tert</i>-butyl-dimethyl-silanyloxy)-2-[3-(<i>tert</i>-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoyl)-amide

Synonyms:propane-2-sulfonic acid (7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoyl)-amide

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Chemical Property of propane-2-sulfonic acid (7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoyl)-amide

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Technology Process of propane-2-sulfonic acid (7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoyl)-amide

There total 2 articles about propane-2-sulfonic acid (7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81363-76-0
propane-2-sulfonamide

: 7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoic acid

: 1026682-12-1
propane-2-sulfonic acid (7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoyl)-amide

Guidance literature:: 7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 0.5h;

propane-2-sulfonamide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.1248/cpb.48.1332

Reference yield:

: 7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoic acid methyl ester

: 1026682-12-1
propane-2-sulfonic acid (7-{3,5-bis-(tert-butyl-dimethyl-silanyloxy)-2-[3-(tert-butyl-dimethyl-silanyloxy)-4-phenylsulfanyl-butyl]-cyclopentyl}-heptanoyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. LiOH / tetrahydrofuran / 20 °C

2.1: CDI / tetrahydrofuran / 0.5 h / 20 °C

2.2: DBU / tetrahydrofuran

With lithium hydroxide; 1,1'-carbonyldiimidazole; In tetrahydrofuran;
DOI:10.1248/cpb.48.1332