((C₆H₅)3PAu)2Os(CO)4

Base Information

Chemical Name:((C₆H₅)3PAu)2Os(CO)4
CAS No.:99747-68-9
Molecular Formula:C₄₀H₃₀Au₂O₄OsP₂
Molecular Weight:1220.76
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)3PAu)2Os(CO)4

Synonyms:((C₆H₅)3PAu)2Os(CO)4

Suppliers and Price of ((C₆H₅)3PAu)2Os(CO)4

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ((C₆H₅)3PAu)2Os(CO)4

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ((C₆H₅)3PAu)2Os(CO)4

There total 4 articles about ((C₆H₅)3PAu)2Os(CO)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl(triphenylphosphine)gold(I)

: 22372-70-9
tetracarbonyldihydroosmium

: 99747-68-9
((C₆H₅)3PAu)2Os(CO)4

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In benzene; byproducts: methane; a benzene soln. of Ph3PAuMe was degassed, H2Os(CO)4 was added under vac. followed by addn. of AIBN as a solid or a benzene soln. under a stream of N2, mixt. was kept at 35°C; reaction mixt. was sampled by quenching the soln. at 0°C and removing of aliquot by syringe under a heavy flow of N2 or Ar; product was identified by its IR spectrum; Kinetics;
DOI:10.1021/ja00265a018

Reference yield:

: methyl(triphenylphosphine)gold(I)

: 22372-70-9
tetracarbonyldihydroosmium

: 99782-58-8
H₂Os(CO)3P(C₆H₅)3

: 99747-68-9
((C₆H₅)3PAu)2Os(CO)4

Guidance literature:: With 2,2'-azobis(isobutyronitrile); triphenylphosphine; In benzene-d6; byproducts: methane; an NMR tube was charged with Ph3PAuMe, PPh3 and AIBN, C6D6 and H2Os(CO)4 were added under vac., sealed tube was heated at 35°C for 2 h; H2Os(CO)3PPh3 to (Ph3PAu)2Os(CO)4 ratio 62:38; (1)H NMR spectral data;
DOI:10.1021/ja00265a018

Reference yield:

: methyl(triphenylphosphine)gold(I)

: 22372-70-9
tetracarbonyldihydroosmium

: 99747-68-9
((C₆H₅)3PAu)2Os(CO)4

: 108-88-3,15644-74-3,16713-13-6
toluene

Guidance literature:: With oxygen; In benzene; byproducts: methane; a benzene soln. of Ph3PAuMe was degassed, H2Os(CO)4 was added under vac., mixt. was kept at 35°C; reaction mixt. was sampled by quenching the soln. at 0°C; product was identified by its IR spectrum;
DOI:10.1021/ja00265a018