octyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

Base Information

• Chemical Name: octyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside
• CAS No.: 1033561-30-6
• Molecular Formula: C₃₅H₅₁NO₁₃
• Molecular Weight: 693.789

Synonyms:octyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

Chemical Property of octyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

Chemical Property:

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Technology Process of octyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

There total 1 articles about octyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

n-octyl 2-acetamido-2-deoxy-4,6-O-benzylidene-α-D-glycopyranoside (1033561-27-1) + ethyl 2,3,4-tri-O-acetyl-1-thio-α-L-rhamnopyranoside (125520-01-6) → octyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside (1033561-30-6)

Guidance literature:

With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; for 0.5h;

DOI:10.1021/jo800457j

Reference yield: 72.0%

octyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside (1033561-30-6) → octyl α-L-rhamnopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside (1033561-32-8)

Guidance literature:

With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 8h; pH=12;

DOI:10.1021/jo800457j

upstream raw materials:

n-octyl 2-acetamido-2-deoxy-4,6-O-benzylidene-α-D-glycopyranoside

ethyl 2,3,4-tri-O-acetyl-1-thio-α-L-rhamnopyranoside

Downstream raw materials:

octyl α-L-rhamnopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

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