Technology Process of (αR)-<α-(3)H1>tyramine hydrochloride
There total 4 articles about (αR)-<α-(3)H1>tyramine hydrochloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / methanol / Heating
2: 1.) lithium aluminium hydride, 2.) ethereal hydrogen chloride / 1.) ether, reflux, 1 h, 2.) methanol
3: 1.) hydrogen, 2.) ethereal hydrogen chloride / 1.) palladium-charcoal / 1.) methanol, 2.) ethanol
With
hydrogenchloride; lithium aluminium tetrahydride; hydrogen; potassium carbonate;
palladium on activated charcoal;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / methanol; H2O / 1 h / 70 °C
2: potassium carbonate / methanol / Heating
3: 1.) lithium aluminium hydride, 2.) ethereal hydrogen chloride / 1.) ether, reflux, 1 h, 2.) methanol
4: 1.) hydrogen, 2.) ethereal hydrogen chloride / 1.) palladium-charcoal / 1.) methanol, 2.) ethanol
With
hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen; potassium carbonate;
palladium on activated charcoal;
In
methanol; water;
- Guidance literature:
-
With
hydrogenchloride; hydrogen;
palladium on activated charcoal;
Yield given. Multistep reaction;
1.) methanol, 2.) ethanol;
