4β-chloro-3(10)-carene

Base Information

• Chemical Name: 4β-chloro-3(10)-carene
• CAS No.: 99530-90-2
• Molecular Formula: C₁₀H₁₅Cl
• Molecular Weight: 170.682

Synonyms:4β-chloro-3(10)-carene

Chemical Property of 4β-chloro-3(10)-carene

Chemical Property:

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Technology Process of 4β-chloro-3(10)-carene

There total 1 articles about 4β-chloro-3(10)-carene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+)-Car-3-ene (498-15-7,19079-29-9) → 2,8-dichloro-p-mentha-1(7),5-diene (112054-87-2) + (+)-3α,4β-dichlorocarane (13837-88-2,30199-18-9,30199-19-0,30199-20-3,38049-05-7,38049-06-8,39067-84-0,99530-91-3) + (-)-3β,4α-dichlorocarane (13837-88-2,30199-18-9,30199-19-0,30199-20-3,38049-05-7,38049-06-8,39067-84-0,99530-91-3) + (-)-4α-chloro-3(10)-carene (13837-87-1,30925-23-6,74514-32-2,99530-90-2)

Guidance literature:

With Perbenzoic acid; isocyanate de chlorosulfonyle; In tetrachloromethane; at 82 ℃; for 1.5h;

DOI:10.1007/BF00953879

Reference yield:

4β-chloro-3(10)-carene (99530-90-2) → 3-carene epoxide (936-91-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 0.58 g / peracetic acid / CHCl₃ / 72 h / 20 °C

2: 0.16 g / LiAlH₄ / diethyl ether

With peracetic acid; lithium aluminium tetrahydride; In diethyl ether; chloroform;

DOI:10.1007/BF00953041

upstream raw materials:

(+)-Car-3-ene

Downstream raw materials:

3-carene epoxide

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