2,2-Dimethyl-5-[3-(4-nitro-phenyl)-[1,4,2]dithiazol-5-ylidene]-[1,3]dioxane-4,6-dione

Base Information

Chemical Name:2,2-Dimethyl-5-[3-(4-nitro-phenyl)-[1,4,2]dithiazol-5-ylidene]-[1,3]dioxane-4,6-dione
CAS No.:117804-90-7
Molecular Formula:C₁₄H₁₀N₂O₆S₂
Molecular Weight:366.375
Hs Code.:

Synonyms:2,2-Dimethyl-5-[3-(4-nitro-phenyl)-[1,4,2]dithiazol-5-ylidene]-[1,3]dioxane-4,6-dione

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Chemical Property of 2,2-Dimethyl-5-[3-(4-nitro-phenyl)-[1,4,2]dithiazol-5-ylidene]-[1,3]dioxane-4,6-dione

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Technology Process of 2,2-Dimethyl-5-[3-(4-nitro-phenyl)-[1,4,2]dithiazol-5-ylidene]-[1,3]dioxane-4,6-dione

There total 3 articles about 2,2-Dimethyl-5-[3-(4-nitro-phenyl)-[1,4,2]dithiazol-5-ylidene]-[1,3]dioxane-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 2033-24-1
cycl-isopropylidene malonate

: C₁₂H₁₂N₃O₂S₂⁽¹⁺⁾*BF₄^(1-)

: 117804-90-7
2,2-Dimethyl-5-[3-(4-nitro-phenyl)-[1,4,2]dithiazol-5-ylidene]-[1,3]dioxane-4,6-dione

Guidance literature:: With triethylamine; In acetonitrile; at 25 ℃; for 2h;

Reference yield:

: 61947-11-3
(E)-N-((methylsulfonyl)oxy)-4-nitrobenzimidoyl chloride

: 117804-90-7
2,2-Dimethyl-5-[3-(4-nitro-phenyl)-[1,4,2]dithiazol-5-ylidene]-[1,3]dioxane-4,6-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / acetone / 5 h / 25 °C

2: 73 percent / 54 percent fluoroboric acid / CHCl₃; diethyl ether / 0.5 h

3: 43 percent / triethylamine / acetonitrile / 2 h / 25 °C

With tetrafluoroboric acid; triethylamine; In diethyl ether; chloroform; acetone; acetonitrile;

Reference yield:

: 117804-43-0
C₁₃H₁₅N₃O₅S₃

: 117804-90-7
2,2-Dimethyl-5-[3-(4-nitro-phenyl)-[1,4,2]dithiazol-5-ylidene]-[1,3]dioxane-4,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 54 percent fluoroboric acid / CHCl₃; diethyl ether / 0.5 h

2: 43 percent / triethylamine / acetonitrile / 2 h / 25 °C

With tetrafluoroboric acid; triethylamine; In diethyl ether; chloroform; acetonitrile;