N-(3-{5-[3-(3-dimethylamino-propylamino)-propyl]-9,9-dimethyl-9H-xanthen-4-yl}-propyl)-N',N'-dimethyl-propane-1,3-diamine

Base Information

Chemical Name:N-(3-{5-[3-(3-dimethylamino-propylamino)-propyl]-9,9-dimethyl-9H-xanthen-4-yl}-propyl)-N',N'-dimethyl-propane-1,3-diamine
CAS No.:289719-94-4
Molecular Formula:C₃₁H₅₀N₄O
Molecular Weight:494.764
Hs Code.:

<i>N</i>-(3-{5-[3-(3-dimethylamino-propylamino)-propyl]-9,9-dimethyl-9<i>H</i>-xanthen-4-yl}-propyl)-<i>N</i>',<i>N</i>'-dimethyl-propane-1,3-diamine

Synonyms:N-(3-{5-[3-(3-dimethylamino-propylamino)-propyl]-9,9-dimethyl-9H-xanthen-4-yl}-propyl)-N',N'-dimethyl-propane-1,3-diamine

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Chemical Property of N-(3-{5-[3-(3-dimethylamino-propylamino)-propyl]-9,9-dimethyl-9H-xanthen-4-yl}-propyl)-N',N'-dimethyl-propane-1,3-diamine

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Technology Process of N-(3-{5-[3-(3-dimethylamino-propylamino)-propyl]-9,9-dimethyl-9H-xanthen-4-yl}-propyl)-N',N'-dimethyl-propane-1,3-diamine

There total 1 articles about N-(3-{5-[3-(3-dimethylamino-propylamino)-propyl]-9,9-dimethyl-9H-xanthen-4-yl}-propyl)-N',N'-dimethyl-propane-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19814-75-6
9,9-dimethylxanthene

: 289719-94-4
N-(3-{5-[3-(3-dimethylamino-propylamino)-propyl]-9,9-dimethyl-9H-xanthen-4-yl}-propyl)-N',N'-dimethyl-propane-1,3-diamine

Guidance literature:: Multi-step reaction with 6 steps

1.1: BuLi; TMEDA

1.2: 72 percent / diethyl ether / 18 h / 25 °C

2.1: 93 percent / CH₂Cl₂ / 1 h / Heating

3.1: 100 percent / H₂ / Pd/C / ethyl acetate / 18 h / 25 °C

4.1: 97 percent / LiAlH₄ / diethyl ether / 0.5 h / 0 °C

5.1: 72 percent / I₂; Ph₃P; imidazole / diethyl ether; acetonitrile / 5 h / 25 °C

6.1: 68 percent / tetrahydrofuran / 1 h / Heating

With 1H-imidazole; lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen; iodine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate; acetonitrile; 1.1: Metallation / 1.2: Formylation / 2.1: Condensation / 3.1: Catalytic hydrogenation / 4.1: Reduction / 5.1: Iodination / 6.1: Condensation;
DOI:10.1016/S0960-894X(00)00154-2