4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride

Base Information

Chemical Name:4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride
CAS No.:1618089-87-4
Molecular Formula:C₃₆H₃₈N₆O₃*ClH
Molecular Weight:639.197
Hs Code.:

Synonyms:4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride

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Chemical Property of 4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride

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Technology Process of 4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride

There total 1 articles about 4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1618089-86-3
ethyl 4-(3,5-bis((bis(pyridin-2-ylmethyl)amino)methyl)phenoxy)butanoate

: 1618089-87-4
4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride

Guidance literature:: ethyl 4-(3,5-bis((bis(pyridin-2-ylmethyl)amino)methyl)phenoxy)butanoate; With sodium hydroxide; In tetrahydrofuran; methanol; water; for 2h; Reflux;

With hydrogenchloride; In tetrahydrofuran; methanol; water; pH=Ca. 7;
DOI:10.1039/c4ob00924j

Reference yield: 86.0%

: C₆₈H₁₃₅N₂O₂₁P*H₃N

: 1618089-87-4
4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride

: C₁₀₄H₁₇₁N₈O₂₃P*H₃N

Guidance literature:: 4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride; With dmap; 2,3,4,5,6-pentafluorophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In chloroform; at 0 - 20 ℃; for 16.5h; Inert atmosphere;

C₆₈H₁₃₅N₂O₂₁P*H₃N; With N-ethyl-N,N-diisopropylamine; In chloroform; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c4ob00924j

Reference yield: 65.0%

: C₄₁H₈₃N₂O₇P

: 1618089-87-4
4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride

: C₁₆₈H₂₉₉N₈O₅₆P*H₃N

Guidance literature:: 4-(3,5-bis((bis(pyridin-2-ylmethyl)ammonio)methyl)phenoxy)butanoate chloride; With dmap; 2,3,4,5,6-pentafluorophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In chloroform; at 0 - 20 ℃; for 16.5h; Inert atmosphere;

C₄₁H₈₃N₂O₇P; With N-ethyl-N,N-diisopropylamine; In chloroform; at 20 ℃; for 24h; Inert atmosphere;

With ammonium hydroxide; In methanol; chloroform; Inert atmosphere;
DOI:10.1039/c4ob00924j