(2R,3S,4S,5S,6R)-2-((2S,3S,4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-octyloxy-tetrahydro-furan-3-yloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

Base Information

Chemical Name:(2R,3S,4S,5S,6R)-2-((2S,3S,4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-octyloxy-tetrahydro-furan-3-yloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol
CAS No.:900523-89-9
Molecular Formula:C₃₃H₄₈O₁₀
Molecular Weight:604.738
Hs Code.:

Synonyms:(2R,3S,4S,5S,6R)-2-((2S,3S,4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-octyloxy-tetrahydro-furan-3-yloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

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Chemical Property of (2R,3S,4S,5S,6R)-2-((2S,3S,4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-octyloxy-tetrahydro-furan-3-yloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

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Technology Process of (2R,3S,4S,5S,6R)-2-((2S,3S,4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-octyloxy-tetrahydro-furan-3-yloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

There total 5 articles about (2R,3S,4S,5S,6R)-2-((2S,3S,4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-octyloxy-tetrahydro-furan-3-yloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 900523-88-8
octyl 2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,5-di-O-benzyl-α-D-arabinofuranoside

: 900523-89-9
(2R,3S,4S,5S,6R)-2-((2S,3S,4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-octyloxy-tetrahydro-furan-3-yloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃;
DOI:10.1139/V06-049

Reference yield:

: 900523-84-4
octyl 2,3-anhydro-5-O-benzyl-α-D-lyxofuranoside

: 900523-89-9
(2R,3S,4S,5S,6R)-2-((2S,3S,4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-octyloxy-tetrahydro-furan-3-yloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / phenylmethanol / 100 °C

2: 87 percent / molecular sieves 4 Angstroem; N-iodosuccinimide; silver triflate / CH₂Cl₂ / 20 °C

3: 83 percent / K₂CO₃ / methanol / 20 °C

With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate; potassium carbonate; In methanol; dichloromethane; benzyl alcohol;
DOI:10.1139/V06-049

Reference yield:

: 900523-83-3
octyl 3,5-di-O-benzyl-α-D-arabinofuranoside

: 900523-89-9
(2R,3S,4S,5S,6R)-2-((2S,3S,4R,5R)-4-Benzyloxy-5-benzyloxymethyl-2-octyloxy-tetrahydro-furan-3-yloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / molecular sieves 4 Angstroem; N-iodosuccinimide; silver triflate / CH₂Cl₂ / 20 °C

2: 83 percent / K₂CO₃ / methanol / 20 °C

With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate; potassium carbonate; In methanol; dichloromethane;
DOI:10.1139/V06-049