2-{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-5-{[2-(hydroxymethyl)phenyl]dimethylsilyl}thiophene

Base Information

Chemical Name:2-{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-5-{[2-(hydroxymethyl)phenyl]dimethylsilyl}thiophene
CAS No.:1239354-34-7
Molecular Formula:C₂₇H₃₆O₃SSi₂
Molecular Weight:496.818
Hs Code.:

Synonyms:2-{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-5-{[2-(hydroxymethyl)phenyl]dimethylsilyl}thiophene

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Chemical Property of 2-{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-5-{[2-(hydroxymethyl)phenyl]dimethylsilyl}thiophene

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Technology Process of 2-{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-5-{[2-(hydroxymethyl)phenyl]dimethylsilyl}thiophene

There total 1 articles about 2-{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-5-{[2-(hydroxymethyl)phenyl]dimethylsilyl}thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 953412-92-5
C₁₈H₂₃BrO₂SSi

: 321903-29-1
1,1-dimethyl-1,3-dihydrobenzo[c][1,2]oxasilole

: 1239354-34-7
2-{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-5-{[2-(hydroxymethyl)phenyl]dimethylsilyl}thiophene

Guidance literature:: C₁₈H₂₃BrO₂SSi; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -40 ℃; Inert atmosphere;

With magnesium bromide ethyl etherate; In tetrahydrofuran; hexane; at -40 ℃; for 0.5h; Inert atmosphere;

1,1-dimethyl-1,3-dihydrobenzo[c][1,2]oxasilole; In tetrahydrofuran; hexane; at -40 - 20 ℃; Inert atmosphere;
DOI:10.1246/bcsj.20090325

Reference yield:

: [2-(acetoxymethyl)phenyl](4-bromophenyl)dimethylsilane

: 1239354-34-7
2-{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-5-{[2-(hydroxymethyl)phenyl]dimethylsilyl}thiophene

: 1239354-41-6
C₃₅H₄₂O₄SSi₂

Guidance literature:: With copper(l) iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; at 75 ℃; for 6h; Inert atmosphere;
DOI:10.1246/bcsj.20090325