4-hydroxy-4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]-1-methylpiperidine

Base Information

Chemical Name:4-hydroxy-4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]-1-methylpiperidine
CAS No.:342889-48-9
Molecular Formula:C₃₂H₃₉NO₂
Molecular Weight:469.667
Hs Code.:

Synonyms:4-hydroxy-4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]-1-methylpiperidine

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Chemical Property of 4-hydroxy-4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]-1-methylpiperidine

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Technology Process of 4-hydroxy-4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]-1-methylpiperidine

There total 1 articles about 4-hydroxy-4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]-1-methylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1445-73-4
1-Methyl-4-piperidone

: 204265-31-6
2-bromo-9,9-dipropyl-7-(4-methoxyphenyl)fluorene

: 342889-48-9
4-hydroxy-4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]-1-methylpiperidine

Guidance literature:: 2-bromo-9,9-dipropyl-7-(4-methoxyphenyl)fluorene; With n-butyllithium; In tetrahydrofuran; at -40 ℃; for 0.5h;

1-Methyl-4-piperidone; In tetrahydrofuran; at -30 - -10 ℃;
DOI:10.1002/jhet.5570380102

Reference yield: 36.0%

: 342889-48-9
4-hydroxy-4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]-1-methylpiperidine

: 342889-55-8
4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]pyridine

Guidance literature:: palladium on activated charcoal; In Diphenylmethane; at 220 - 240 ℃; for 18h;
DOI:10.1002/jhet.5570380102

Reference yield:

: 342889-48-9
4-hydroxy-4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]-1-methylpiperidine

: 4-[7-(4-methoxyphenyl)-9,9-dipropylfluoren-2-yl]-1-sulfopropylpyridinium zwitterion

Guidance literature:: Multi-step reaction with 2 steps

1: 36 percent / 10 percent Pd/C / diphenylmethane / 18 h / 220 - 240 °C

2: 0.63 g / benzonitrile / 0.5 h / 180 °C

palladium on activated charcoal; In Diphenylmethane; benzonitrile;
DOI:10.1002/jhet.5570380102