[PhP(CH₂SiMe₂NSiMe₂CH₂)2PPh]NbCl

Base Information

Chemical Name:[PhP(CH₂SiMe₂NSiMe₂CH₂)2PPh]NbCl
CAS No.:477332-53-9
Molecular Formula:C₂₄H₄₂ClN₂NbP₂Si₄
Molecular Weight:661.26
Hs Code.:

[PhP(CH<sub>2</sub>SiMe<sub>2</sub>NSiMe<sub>2</sub>CH<sub>2</sub>)2PPh]NbCl

Synonyms:[PhP(CH₂SiMe₂NSiMe₂CH₂)2PPh]NbCl

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Chemical Property of [PhP(CH₂SiMe₂NSiMe₂CH₂)2PPh]NbCl

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Technology Process of [PhP(CH₂SiMe₂NSiMe₂CH₂)2PPh]NbCl

There total 4 articles about [PhP(CH₂SiMe₂NSiMe₂CH₂)2PPh]NbCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 110615-13-9
niobium(III) chloride dimethoxyethane

: (C₆H₅P(CH₂Si(CH₃)2NSi(CH₃)2CH₂)2PC₆H₅)Li₂(OC₄H₈O)

: 477332-53-9
(PhP(CH₂CSiMe₂NSiMe₂CH₂)2PPh)NbCl

Guidance literature:: In toluene; mixt. Ph(P2N2)Li2(dioxane) and NbCl3(DME) was suspended in toluene and stirred for 2 days; soln. evapd. to dryness, extd. into toluene and filtered, toluene was removed in vacuo, residue was washed with hexane and crystd. from toluene;elem. anal.;
DOI:10.1021/om010356z

Reference yield:

: [(PhP(CH2SiMe2NSiMe2CH2)2PPh)Nb]2(μ-N2)

: 477332-53-9
[PhP(CH₂SiMe₂NSiMe₂CH₂)2PPh]NbCl

Guidance literature:: With PbCl₂; In toluene; byproducts: Pb, N2; PbCl2 was added to a soln. of complex in toluene, the mixt. was stirred for 12 h; soln. was filtered, toluene was removed in vac.;
DOI:10.1021/ja025997f