1-cyclohexylphthalazine

Base Information

Chemical Name:1-cyclohexylphthalazine
CAS No.:137634-68-5
Molecular Formula:C₁₄H₁₆N₂
Molecular Weight:212.294
Hs Code.:

Synonyms:1-cyclohexylphthalazine

Suppliers and Price of 1-cyclohexylphthalazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-cyclohexylphthalazine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

MSDS Files:

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Technology Process of 1-cyclohexylphthalazine

There total 9 articles about 1-cyclohexylphthalazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 253-52-1
PHTHALAZINE

: 110-82-7,25012-93-5
cyclohexane

: 1,4‐dicyclohexylphthalazine

: 137634-68-5
1-cyclohexylphthalazine

Guidance literature:: With dipotassium peroxodisulfate; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; trifluoroacetic acid; In acetonitrile; at 20 ℃; for 16h; Irradiation; Inert atmosphere;
DOI:10.1021/acs.joc.9b01603

Reference yield: 51.0%

: 253-52-1
PHTHALAZINE

: 4441-56-9
cyclohexylboronic acid

: 137634-68-5
1-cyclohexylphthalazine

Guidance literature:: With [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; oxygen; trifluoroacetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 24h; Sealed tube; Irradiation;
DOI:10.1039/d0cc05946c

Reference yield: 46.0%

: 253-52-1
PHTHALAZINE

: 108-85-0
1-bromocyclohexane

: 137634-68-5
1-cyclohexylphthalazine

Guidance literature:: With tris-(trimethylsilyl)silane; [Ir[2-(2,4-difluorophenyl)-5-trifluoromethylpyridine]₂(4,4′-di-t-Bu-2,2′-bipyridine)]PF₆; oxygen; trifluoroacetic acid; In acetone; at 20 ℃; for 24h; regioselective reaction; Irradiation;
DOI:10.1039/c8sc04892d