(R)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide

Base Information

Chemical Name:(R)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide
CAS No.:1092722-90-1
Molecular Formula:C₂₁H₂₁ClNOP
Molecular Weight:369.831
Hs Code.:

Synonyms:(R)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide

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Technology Process of (R)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide

There total 4 articles about (R)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1092722-90-1
(R)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide

Guidance literature:

Reference yield:

: 849940-62-1
C₁₉H₁₅ClNOP

: 557-20-0
diethylzinc

: 1092722-90-1
(R)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide

: (S)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide

: 1224953-91-6
N-(3-chlorobenzyl)-P,P-diphenylphosphinic amide

Guidance literature:: C₁₉H₁₅ClNOP; With methanol; (1S,2R,4R)-N-benzyl-1-amino-2-exo-hydroxy-7,7-dimethyl-bicyclo[2.2.1]heptane; In toluene; at 28 ℃; for 0.166667h; Inert atmosphere;

diethylzinc; In hexane; toluene; at 0 - 28 ℃; for 43h; enantioselective reaction; Inert atmosphere;
DOI:10.1002/asia.201403240

Reference yield:

: 849940-62-1
C₁₉H₁₅ClNOP

: 557-20-0
diethylzinc

: 1092722-90-1
(R)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide

: (S)-N-[1-(3-chlorophenyl)propyl]-P,P-diphenylphosphinoylamide

Guidance literature:: C₁₉H₁₅ClNOP; With (1S,2R,4R)-7,7-dimethyl-1-morpholin-4-yl-bicyclo[2.2.1]heptan-2-ol; In toluene; at 28 ℃; for 0.166667h; Inert atmosphere;

diethylzinc; In hexane; toluene; at 0 - 28 ℃; for 30h; Overall yield = 84 %; Overall yield = 105.6 mg; enantioselective reaction; Inert atmosphere;
DOI:10.1002/asia.201403240