methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside
CAS No.:634613-20-0
Molecular Formula:C₅₅H₆₀O₁₁
Molecular Weight:897.075
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

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Chemical Property of methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

There total 4 articles about methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1096120-24-9
methyl 6-O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 634613-20-0
methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

Guidance literature:: methyl 6-O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranoside; With methanol; sodium methylate; In dichloromethane; at 20 ℃; for 1h;

With Amberlite IR-120; In methanol; dichloromethane;
DOI:10.1021/jo8019835

Reference yield:

: C₅₇H₆₂O₁₂

: 634613-20-0
methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

: C₅₅H₆₀O₁₁

Guidance literature:: With methanol; sodium methylate; In tetrahydrofuran; at 20 ℃;
DOI:10.1246/BCSJ.20200305

Reference yield:

: 186540-10-3
methyl 2,3,4-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 634613-20-0
methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

: C₅₅H₆₀O₁₁

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 4 - 20 °C

2: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / -40 - -20 °C / Molecular sieve

3: sodium methylate; methanol / tetrahydrofuran / 20 °C

With pyridine; methanol; N-iodo-succinimide; trifluorormethanesulfonic acid; sodium methylate; In tetrahydrofuran; dichloromethane;
DOI:10.1246/BCSJ.20200305