2,2'-diethyl-6,6'-dihydroxy-2,2'-bis(4-(methoxy)benzyloxy)-bicyclohexyl-4,4'-diene-3,3'-dione

Base Information

Chemical Name:2,2'-diethyl-6,6'-dihydroxy-2,2'-bis(4-(methoxy)benzyloxy)-bicyclohexyl-4,4'-diene-3,3'-dione
CAS No.:1403821-12-4
Molecular Formula:C₃₂H₃₈O₈
Molecular Weight:550.649
Hs Code.:

Synonyms:2,2'-diethyl-6,6'-dihydroxy-2,2'-bis(4-(methoxy)benzyloxy)-bicyclohexyl-4,4'-diene-3,3'-dione

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Chemical Property of 2,2'-diethyl-6,6'-dihydroxy-2,2'-bis(4-(methoxy)benzyloxy)-bicyclohexyl-4,4'-diene-3,3'-dione

Chemical Property:

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Technology Process of 2,2'-diethyl-6,6'-dihydroxy-2,2'-bis(4-(methoxy)benzyloxy)-bicyclohexyl-4,4'-diene-3,3'-dione

There total 9 articles about 2,2'-diethyl-6,6'-dihydroxy-2,2'-bis(4-(methoxy)benzyloxy)-bicyclohexyl-4,4'-diene-3,3'-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1403821-22-6
C₃₂H₃₈O₁₀

: 1403821-12-4
2,2'-diethyl-6,6'-dihydroxy-2,2'-bis(4-(methoxy)benzyloxy)-bicyclohexyl-4,4'-diene-3,3'-dione

Guidance literature:: With triphenylphosphine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol302567f

Reference yield:

: C₄₄H₆₆O₆Si₂

: 1403821-12-4
2,2'-diethyl-6,6'-dihydroxy-2,2'-bis(4-(methoxy)benzyloxy)-bicyclohexyl-4,4'-diene-3,3'-dione

Guidance literature:: Multi-step reaction with 3 steps

1: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 0.75 h / -78 °C / Inert atmosphere; Irradiation

2: fluorosilicic acid / acetonitrile / 0.67 h / 0 °C / Inert atmosphere

3: triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With fluorosilicic acid; oxygen; 5,15,10,20-tetraphenylporphyrin; triphenylphosphine; In dichloromethane; acetonitrile;
DOI:10.1021/ol302567f

Reference yield:

: 1403821-21-5
1,1'-bis-(tert-butyl(dimethyl)silanyloxy)-6,6'-diethyl-6,6'-bis-(4-(methoxy)benzyloxy)-[5,5']bi[2,3-dioxabicyclo[2.2.2]octyl]-7,7'-diene

: 1403821-12-4
2,2'-diethyl-6,6'-dihydroxy-2,2'-bis(4-(methoxy)benzyloxy)-bicyclohexyl-4,4'-diene-3,3'-dione

Guidance literature:: Multi-step reaction with 2 steps

1: fluorosilicic acid / acetonitrile / 0.67 h / 0 °C / Inert atmosphere

2: triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With fluorosilicic acid; triphenylphosphine; In dichloromethane; acetonitrile;
DOI:10.1021/ol302567f