phenyl-carbamic acid 4-(3,4-bis-ethylsulfanyl-2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzyl ester

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Chemical Name:phenyl-carbamic acid 4-(3,4-bis-ethylsulfanyl-2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzyl ester
CAS No.:1451073-36-1
Molecular Formula:C₂₂H₂₂N₂O₄S₂
Molecular Weight:442.56
Hs Code.:

Synonyms:phenyl-carbamic acid 4-(3,4-bis-ethylsulfanyl-2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzyl ester

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Chemical Property of phenyl-carbamic acid 4-(3,4-bis-ethylsulfanyl-2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzyl ester

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Technology Process of phenyl-carbamic acid 4-(3,4-bis-ethylsulfanyl-2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzyl ester

There total 2 articles about phenyl-carbamic acid 4-(3,4-bis-ethylsulfanyl-2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1451073-35-0
3,4-bis-ethylsulfanyl-1-(4-hydroxymethyl-phenyl)-pyrrole-2,5-dione

: 103-71-9
phenyl isocyanate

: 1451073-36-1
phenyl-carbamic acid 4-(3,4-bis-ethylsulfanyl-2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1039/c3cc45220d

Reference yield:

: 1442447-57-5
3,4-dibromo-1-(4-hydroxymethyl-phenyl)-pyrrole-2,5-dione

: 1451073-36-1
phenyl-carbamic acid 4-(3,4-bis-ethylsulfanyl-2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 20 °C

2: triethylamine / dichloromethane / 48 h / 20 °C

With triethylamine; In dichloromethane;
DOI:10.1039/c3cc45220d