[4-(2,6-Dioxo-1,3-dipropyl-2,3,6,9-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid hydrazide

Base Information

Chemical Name:[4-(2,6-Dioxo-1,3-dipropyl-2,3,6,9-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid hydrazide
CAS No.:96865-94-0
Molecular Formula:C₁₉H₂₄N₆O₄
Molecular Weight:400.437
Hs Code.:

Synonyms:[4-(2,6-Dioxo-1,3-dipropyl-2,3,6,9-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid hydrazide

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Chemical Property of [4-(2,6-Dioxo-1,3-dipropyl-2,3,6,9-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid hydrazide

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Technology Process of [4-(2,6-Dioxo-1,3-dipropyl-2,3,6,9-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid hydrazide

There total 5 articles about [4-(2,6-Dioxo-1,3-dipropyl-2,3,6,9-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 96865-87-1
8-<4-<(carboxymethyl)oxy>phenyl>-1,3-dipropylxanthine ethyl ester

: 96865-94-0
[4-(2,6-Dioxo-1,3-dipropyl-2,3,6,9-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid hydrazide

Guidance literature:: With hydrazine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00147a038

Reference yield:

: 81250-34-2
1,3-dipropyl-5,6-diaminouracil

: 96865-94-0
[4-(2,6-Dioxo-1,3-dipropyl-2,3,6,9-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / acetic acid / methanol / 0.25 h / Heating

2: 71 percent / ferric chloride / 24 h / Heating

3: 90 percent / N₂H₄ / dimethylformamide

With iron(III) chloride; acetic acid; hydrazine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00147a038

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 96865-94-0
[4-(2,6-Dioxo-1,3-dipropyl-2,3,6,9-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / potassium carbonate / dimethylformamide / 72 h / 60 °C

2: 86 percent / acetic acid / methanol / 0.25 h / Heating

3: 71 percent / ferric chloride / 24 h / Heating

4: 90 percent / N₂H₄ / dimethylformamide

With iron(III) chloride; potassium carbonate; acetic acid; hydrazine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00147a038