(5R)-5-methyl-3-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-2,4-imidazolidinedione

Base Information

Chemical Name:(5R)-5-methyl-3-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-2,4-imidazolidinedione
CAS No.:1311136-63-6
Molecular Formula:C₁₇H₁₆N₂O₄
Molecular Weight:312.325
Hs Code.:

Synonyms:(5R)-5-methyl-3-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-2,4-imidazolidinedione

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Chemical Property of (5R)-5-methyl-3-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-2,4-imidazolidinedione

Chemical Property:

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Technology Process of (5R)-5-methyl-3-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-2,4-imidazolidinedione

There total 3 articles about (5R)-5-methyl-3-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-2,4-imidazolidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32315-10-9
bis(trichloromethyl) carbonate

: 1311137-75-3
N'-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-D-alaninamide

: 1311136-63-6
(5R)-5-methyl-3-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-2,4-imidazolidinedione

Guidance literature:: bis(trichloromethyl) carbonate; N'-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-D-alaninamide; With triethylamine; In ethyl acetate; for 0.0833333h;

With dmap; In ethyl acetate; for 0.166667h;

Reference yield:

: 56705-86-3
4-(3-methoxyphenoxy)aniline

: 1311136-63-6
(5R)-5-methyl-3-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-2,4-imidazolidinedione

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.25 h / 20 °C

1.2: 0.5 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3.1: triethylamine / ethyl acetate / 0.08 h

3.2: 0.17 h

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1311137-74-2
1,1-dimethylethyl {(1R)-1-methyl-2-[(4-{[3-(methyloxy)phenyl]oxy}phenyl)amino]-2-oxoethyl}carbamate

: 1311136-63-6
(5R)-5-methyl-3-(4-{[3-(methyloxy)phenyl]oxy}phenyl)-2,4-imidazolidinedione

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2.1: triethylamine / ethyl acetate / 0.08 h

2.2: 0.17 h

With triethylamine; trifluoroacetic acid; In dichloromethane; ethyl acetate;