(E)-1,2-dideuterio-1-(phenylsulfonyl)-2-(trimethylsilyl)ethylene

Base Information

• Chemical Name: (E)-1,2-dideuterio-1-(phenylsulfonyl)-2-(trimethylsilyl)ethylene
• CAS No.: 82201-53-4
• Molecular Formula: C₁₁H₁₆O₂SSi
• Molecular Weight: 242.382
• Mol file: 82201-53-4.mol

Synonyms:(E)-1,2-dideuterio-1-(phenylsulfonyl)-2-(trimethylsilyl)ethylene

Chemical Property of (E)-1,2-dideuterio-1-(phenylsulfonyl)-2-(trimethylsilyl)ethylene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (E)-1,2-dideuterio-1-(phenylsulfonyl)-2-(trimethylsilyl)ethylene

There total 1 articles about (E)-1,2-dideuterio-1-(phenylsulfonyl)-2-(trimethylsilyl)ethylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

1-(Phenylsulfonyl)-2-(trimethylsilyl)acetylene (32501-93-2) → (E)-1,2-dideuterio-1-(phenylsulfonyl)-2-(trimethylsilyl)ethylene (82201-53-4)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 36h; under 1861.7 Torr; Ambient temperature;

DOI:10.1021/jo00173a039

Reference yield: 96.5%

anthracene (120-12-7) + (E)-1,2-dideuterio-1-(phenylsulfonyl)-2-(trimethylsilyl)ethylene (82201-53-4) → C25H24(2)H2O2SSi (87585-84-0)

Guidance literature:

In toluene; at 160 ℃; for 228h;

DOI:10.1021/jo00173a039

upstream raw materials:

1-(Phenylsulfonyl)-2-(trimethylsilyl)acetylene

Downstream raw materials:

C₂₅H₂₄⁽²⁾H₂O₂SSi