Benzo(c)phenanthrene-5,6-imine

Base Information

Chemical Name:Benzo(c)phenanthrene-5,6-imine
CAS No.:71382-54-2
Molecular Formula:C₁₈H₁₃N
Molecular Weight:243.308
Hs Code.:
DSSTox Substance ID:DTXSID70991719
Nikkaji Number:J590.804C
Mol file:71382-54-2.mol

Synonyms:5,5a-dihydro-4bh-benzo[3,4]phenanthro[1,2-b]azirene;DTXSID70991719;3-azapentacyclo[9.8.0.02,4.05,10.012,17]nonadeca-1(11),5,7,9,12,14,16,18-octaene

Suppliers and Price of Benzo(c)phenanthrene-5,6-imine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BENZO(C)PHENANTHRENE-5,6-IMINE 95.00%
5MG
$ 505.32

Total 3 raw suppliers

Chemical Property of Benzo(c)phenanthrene-5,6-imine

Chemical Property:

Vapor Pressure:4.98E-08mmHg at 25°C
Boiling Point:442.5°C at 760 mmHg
Flash Point:244.4°C
PSA：21.94000
Density:1.247g/cm³
LogP:4.53460
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:243.104799419
Heavy Atom Count:19
Complexity:365

Purity/Quality:

99% ^*data from raw suppliers

BENZO(C)PHENANTHRENE-5,6-IMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC3=C2C4=CC=CC=C4C5C3N5

Technology Process of Benzo(c)phenanthrene-5,6-imine

There total 2 articles about Benzo(c)phenanthrene-5,6-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60692-90-2,100017-08-1,100017-09-2
Benzophenanthrene 5,6-oxide

: 71382-54-2
benzophenanthrene-5,6-imine

Guidance literature:: With lithium aluminium tetrahydride; thionyl chloride; Yield given. Multistep reaction;

Reference yield:

: 71382-61-1
1-phenylnaphthalene-2,2'-dicarboxaldehyde

: 71382-54-2
benzophenanthrene-5,6-imine

Guidance literature:: Multi-step reaction with 2 steps

2: 2.) SOCl₂, 3.) LiAlH₄

With lithium aluminium tetrahydride; thionyl chloride;