(+/-)-Verbascenine

Base Information

Chemical Name:(+/-)-Verbascenine
CAS No.:87554-71-0
Molecular Formula:C₃₀H₄₀N₄O₃
Molecular Weight:504.673
Hs Code.:

Synonyms:(+/-)-Verbascenine

Suppliers and Price of (+/-)-Verbascenine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 0 raw suppliers

Chemical Property of (+/-)-Verbascenine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (+/-)-Verbascenine

There total 26 articles about (+/-)-Verbascenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 108-24-7
acetic anhydride

: 174393-34-1
(+/-)-verbacine

: 87554-71-0
(+/-)-Verbascenine

Guidance literature:: With triethylamine; In dichloromethane; at -78 ℃;
DOI:10.1021/ja953541a

Reference yield: 58.0%

: 87499-87-4
13-Acetyl-8-phenyl-1,5,9,13-tetraaza-cycloheptadecan-6-one

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 87554-71-0
(+/-)-Verbascenine

Guidance literature:: With dmap; triethylamine; at -78 ℃;
DOI:10.1016/S0040-4039(00)88197-6

Reference yield:

: 71-44-3
Spermine

: 87554-71-0
(+/-)-Verbascenine

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) H₂, CHCl₃ / 2.) PtO₂

2: 90 percent / Sb(OEt)3 / benzene / 9 h / 80 °C

3: 1.) (3,5-bis(trifluoromethyl)phenyl)boronic acid / 1.) CH₂Cl₂, from -78 deg C to RT, 2.) CH₂Cl₂, -78 deg C

4: 91 percent / triethylamine / CH₂Cl₂ / -78 °C

With chloroform; triethoxyantimony; hydrogen; triethylamine; 3,5-bis-trifluromethylphenylboronic acid; platinum(IV) oxide; In dichloromethane; benzene;
DOI:10.1021/ja953541a