Technology Process of C26H38O6Si
There total 7 articles about C26H38O6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver tetrafluoroborate;
In
benzene;
at 80 ℃;
for 1.45h;
Darkness;
DOI:10.1021/ja404796n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: AD-mix β; methanesulfonamide / tert-butyl alcohol; water / 40 h / 0 °C
2: silver tetrafluoroborate / benzene / 1.45 h / 80 °C / Darkness
With
silver tetrafluoroborate; methanesulfonamide; AD-mix β;
In
water; tert-butyl alcohol; benzene;
DOI:10.1021/ja404796n
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C
2.1: pyridine / dichloromethane / 1.5 h / 0 °C
2.2: 2.5 h / 0 - 20 °C
3.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 2.75 h / 20 °C
4.1: AD-mix β; methanesulfonamide / tert-butyl alcohol; water / 40 h / 0 °C
5.1: silver tetrafluoroborate / benzene / 1.45 h / 80 °C / Darkness
With
pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; silver tetrafluoroborate; methanesulfonamide; AD-mix β; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol; benzene;
3.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ja404796n