4-O-benzyl-3-O-(2-butenyl)-6-O-(tert-butyldiphenylsilyl)-2-O-(p-nitrobenzoyl)-α-D-glucopyranosyl chloride

Base Information

Chemical Name:4-O-benzyl-3-O-(2-butenyl)-6-O-(tert-butyldiphenylsilyl)-2-O-(p-nitrobenzoyl)-α-D-glucopyranosyl chloride
CAS No.:83158-16-1
Molecular Formula:C₄₀H₄₄ClNO₈Si
Molecular Weight:730.33
Hs Code.:

Synonyms:4-O-benzyl-3-O-(2-butenyl)-6-O-(tert-butyldiphenylsilyl)-2-O-(p-nitrobenzoyl)-α-D-glucopyranosyl chloride

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Chemical Property of 4-O-benzyl-3-O-(2-butenyl)-6-O-(tert-butyldiphenylsilyl)-2-O-(p-nitrobenzoyl)-α-D-glucopyranosyl chloride

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Technology Process of 4-O-benzyl-3-O-(2-butenyl)-6-O-(tert-butyldiphenylsilyl)-2-O-(p-nitrobenzoyl)-α-D-glucopyranosyl chloride

There total 7 articles about 4-O-benzyl-3-O-(2-butenyl)-6-O-(tert-butyldiphenylsilyl)-2-O-(p-nitrobenzoyl)-α-D-glucopyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 83158-15-0
C₄₇H₄₈N₂O₁₂Si

: 83158-16-1
4-O-benzyl-3-O-(2-butenyl)-6-O-(tert-butyldiphenylsilyl)-2-O-(p-nitrobenzoyl)-α-D-glucopyranosyl chloride

Guidance literature:: With hydrogenchloride; In diethyl ether;
DOI:10.1016/S0008-6215(00)82602-6

Reference yield:

: 83158-09-2
Acetic acid (4aR,7R,8S,8aR)-6-acetoxy-8-[((E)-but-2-enyl)oxy]-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

: 83158-16-1
4-O-benzyl-3-O-(2-butenyl)-6-O-(tert-butyldiphenylsilyl)-2-O-(p-nitrobenzoyl)-α-D-glucopyranosyl chloride

Guidance literature:: Multi-step reaction with 7 steps

1: 70 percent / silver oxide

2: 90 percent

3: 90 percent / imidazole

4: tris(triphenylphosphine)-rhodium(II) chloride

5: 60 percent / mercuric chloride

6: 80 percent

7: 70 percent / hydrogen chloride / diethyl ether

With 1H-imidazole; hydrogenchloride; Wilkinson's catalyst; mercury dichloride; silver(l) oxide; In diethyl ether;
DOI:10.1016/S0008-6215(00)82602-6

Reference yield:

: 83158-11-6
{(2R,3R,4S,5R)-5,6-Bis-allyloxy-3-benzyloxy-4-[((E)-but-2-enyl)oxy]-tetrahydro-pyran-2-yl}-methanol

: 83158-16-1
4-O-benzyl-3-O-(2-butenyl)-6-O-(tert-butyldiphenylsilyl)-2-O-(p-nitrobenzoyl)-α-D-glucopyranosyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / imidazole

2: tris(triphenylphosphine)-rhodium(II) chloride

3: 60 percent / mercuric chloride

4: 80 percent

5: 70 percent / hydrogen chloride / diethyl ether

With 1H-imidazole; hydrogenchloride; Wilkinson's catalyst; mercury dichloride; In diethyl ether;
DOI:10.1016/S0008-6215(00)82602-6