N-<2-(N-Z)aminoethyl>-N-glycine

Base Information

Chemical Name:N-<2-(N-Z)aminoethyl>-N-glycine
CAS No.:221554-80-9
Molecular Formula:C₁₆H₂₀N₂O₆
Molecular Weight:336.345
Hs Code.:

Synonyms:N-<2-(N-Z)aminoethyl>-N-glycine

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Chemical Property of N-<2-(N-Z)aminoethyl>-N-glycine

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Technology Process of N-<2-(N-Z)aminoethyl>-N-glycine

There total 1 articles about N-<2-(N-Z)aminoethyl>-N-glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 221554-78-5
methyl N-<2-(N-Z)aminoethyl>-N-glycinate

: 221554-80-9
N-<2-(N-Z)aminoethyl>-N-glycine

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1016/S0040-4020(98)01211-3

Reference yield:

: 221554-80-9
N-<2-(N-Z)aminoethyl>-N-glycine

: 221554-89-8
{Allyloxycarbonyl-[2-(2-{(2-{2-[allyloxycarbonyl-(2-benzyloxycarbonylamino-ethyl)-amino]-acetylamino}-ethyl)-[2-(2-amino-6-benzyloxy-purin-9-yl)-acetyl]-amino}-acetylamino)-ethyl]-amino}-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) isobutyl chloroformate, 2.) Et₃N / 1.) CH₂Cl₂, -15 deg C, 15 min, 2.) CH₂Cl₂, -15 deg C (3 h), -> room temperature (1 h)

2: 90 percent / aq. LiOH / methanol / 2 h / 0 °C

3: 1.) isobutyl chloroformate, 2.) Et₃N / 1.) CH₂Cl₂, -15 deg C, 15 min, 2.) CH₂Cl₂, -15 deg C (3 h) -> room temperature (1 h)

4: 95 percent / Cd, AcOH / dimethylformamide / 2 h / Ambient temperature

5: 90 percent / Brop / CH₂Cl₂ / 18 h / 0 °C

With lithium hydroxide; bromo-tris-dimethylamino-phosphonium hexafluorophosphate; acetic acid; triethylamine; cadmium; isobutyl chloroformate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(98)01211-3

Reference yield:

: 221554-80-9
N-<2-(N-Z)aminoethyl>-N-glycine

: 221554-85-4
[(2-{2-[allyloxycarbonyl-(2-benzyloxycarbonylamino-ethyl)-amino]-acetylamino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) isobutyl chloroformate, 2.) Et₃N / 1.) CH₂Cl₂, -15 deg C, 15 min, 2.) CH₂Cl₂, -15 deg C (3 h), -> room temperature (1 h)

2: 90 percent / aq. LiOH / methanol / 2 h / 0 °C

With lithium hydroxide; triethylamine; isobutyl chloroformate; In methanol;
DOI:10.1016/S0040-4020(98)01211-3